Displaying publications 61 - 80 of 364 in total

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  1. Green synthesis of silver nanoparticles using Ocimum sanctum Linn. and its antibacterial activity against multidrug resistant Acinetobacter baumannii
    Gautam D, Dolma KG, Khandelwal B, Gupta M, Singh M, Mahboob T, et al.
    PeerJ, 2023;11:e15590.
    PMID: 37529215 DOI: 10.7717/peerj.15590
    The biosynthesis of nanoparticles using the green route is an effective strategy in nanotechnology that provides a cost-effective and environmentally friendly alternative to physical and chemical methods. This study aims to prepare an aqueous extract of Ocimum sanctum (O. sanctum)-based silver nanoparticles (AgNPs) through the green route and test their antibacterial activity. The biosynthesized silver nanoparticles were characterised by colour change, UV spectrometric analysis, FTIR, and particle shape and size morphology by SEM and TEM images. The nanoparticles are almost spherical to oval or rod-shaped with smooth surfaces and have a mean particle size in the range of 55 nm with a zeta potential of -2.7 mV. The antibacterial activities of AgNPs evaluated against clinically isolated multidrug-resistant Acinetobacter baumannii (A. baumannii) showed that the AgNPs from O. sanctum are effective in inhibiting A. baumannii growth with a zone of inhibition of 15 mm in the agar well diffusion method and MIC and MBC of 32 µg/mL and 64 µg/mL, respectively. The SEM images of A. baumannii treated with AgNPs revealed damage and rupture in bacterial cells. The time-killing assay by spectrophotometry revealed the time- and dose-dependent killing action of AgNPs against A. baumannii, and the assay at various concentrations and time intervals indicated a statistically significant result in comparison with the positive control colistin at 2 µg/mL (P 
    Matched MeSH terms: Silver/pharmacology
  2. Green synthesis and characterization of silver and copper nanoparticles and their use as an effective adsorbent for chromium removal and recovery from wastewater
    Irshad MA, Sattar S, Al-Huqail AA, Alghanem SMS, Nawaz R, Ain NU, et al.
    Environ Sci Pollut Res Int, 2023 Nov;30(52):112575-112590.
    PMID: 37833594 DOI: 10.1007/s11356-023-30141-3
    Chromium (Cr) is one of the hazardous heavy metals that is naturally carcinogenic and causes various health problems. Metallic nanoparticles such as silver and copper nanoparticles (Ag NPs and Cu NPs) have gained great attention because of their unique chemical, physical, and biological attributes, serving diverse and significant role in various useful and sustainable applications. In the present study, both of these NPs were synthesized by green method in which Azadirachta indica plant extract was used. These nanoparticles were characterized by using advanced instrumental techniques such as Fourier transmission infrared (FTIR), X-ray diffraction (XRD), scanning electron microscope attached with energy-dispersive spectroscopy (SEM-EDS), and elemental mapping. These environmentally friendly nanoparticles were utilized for the batch removal of Cr from the wastewater. For analysis of adsorption behaviour, a range of kinetic isotherm models (Freundlich, Temkin, Dubinin, and Langmuir) and kinetic models (pseudo-first-order and pseudo-second-order) were used for the Cu-NPs and Ag-NPs. Cu NPs exhibited the highest Cr removal efficiency (96%) within a contact time of 10-15 min, closely followed by Ag NPs which achieved a removal efficiency of 94% under the similar conditions. These optimal outcomes were observed at a sorbent dose of 0.5 g/L for Ag NPs and 0.7 g/L for Cu NPs. After effectively capturing Cr using these nanoparticles, the sorbates were examined through SEM-EDX analysis to observe how much Cr metal was attached to the nanoparticles, potentially for future use. The analysis found that Ag-NPs captured 18% of Cr, while Cu-NPs captured 12% from the aqueous solution. More precise experimental conditions are needed for higher Cr removal from wastewater and determination of the best conditions for industrial-level Cr reuse. Although nanomaterial exhibit high efficiency and selectivity for Cr removal and recovery from wastewater, more research is necessary to optimize their synthesis and performance for industrial-scale applications and develop efficient methods for Cr removal and recovery.
    Matched MeSH terms: Silver/chemistry
  3. Fulltext Low concentration of silver nanoparticles not only enhances the activity of horseradish peroxidase but alter the structure also
    Karim Z, Adnan R, Ansari MS
    PLoS One, 2012;7(7):e41422.
    PMID: 22848490 DOI: 10.1371/journal.pone.0041422
    Chemical synthesis of Ag-NPs was carried out using reduction method. The reduction mechanistic approach of silver ions was found to be a basic clue for the formation of the Ag-NPs. The nanoparticles were characterized by UV-vis, FT-IR and TEM analysis. We had designed some experiments in support of our hypothesis, "low concentrations of novel nanoparticles (silver and gold) increases the activity of plant peroxidases and alter their structure also", we had used Ag-NPs and HRP as models. The immobilization/interaction experiment had demonstrated the specific concentration range of the Ag-NPs and within this range, an increase in HRP activity was reported. At 0.08 mM concentration of Ag-NPs, 50% increase in the activity yield was found. The U.V-vis spectra had demonstrated the increase in the absorbance of HRP within the reported concentration range (0.06-0.12 mM). Above and below this concentration range there was a decrease in the activity of HRP. The results that we had found from the fluorescence spectra were also in favor of our hypothesis. There was a maximum increase in ellipticity and α-helix contents in the presence of 0.08 mM concentration of Ag-NPs, demonstrated by circular dichroism (CD) spectra. Finally, incubation of a plant peroxidase, HRP with Ag-NPs, within the reported concentration range not only enhances the activity but also alter the structure.
    Matched MeSH terms: Silver/chemistry*
  4. Fulltext Investigation of graphene-on-metal substrates for SPR-based sensor using finite-difference time domain
    Said FA, Menon PS, Rajendran V, Shaari S, Majlis BY
    IET Nanobiotechnol, 2017 Dec;11(8):981-986.
    PMID: 29155398 DOI: 10.1049/iet-nbt.2017.0051
    In this study, the authors investigated the effects of a single layer graphene as a coating layer on top of metal thin films such as silver, gold, aluminum and copper using finite-difference time domain method. To enhance the resolution of surface plasmon resonance (SPR) sensor, it is necessary to increase the SPR reflectivity and decrease the full-width-half maximum (FWHM) of the SPR curve so that there is minimum uncertainty in the determination of the resonance dip. Numerical data was verified with analytical and experimental data where all the data were in good agreement with resonance angle differing in <10% due to noise present in components such as humidity and temperature. In further analysis, reflectivity and FWHM were compared among four types of metal with various thin film thicknesses where graphene was applied on top of the metal layers, and data was compared against pure conventional metal thin films. A 60 nm-thick Au thin film results in higher performance with reflectivity of 92.4% and FWHM of 0.88° whereas single layer graphene-on-60 nm-thick Au gave reflectivity of 91.7% and FWHM of 1.32°. However, a graphene-on-40 nm-thick Ag also gave good performance with narrower FWHM of 0.88° and reflection spectra of 89.2%.
    Matched MeSH terms: Silver/chemistry*
  5. Synthesis of poly(3-hydroxybutyrate-co-4-hydroxybutyrate)/chitosan/silver nanocomposite material with enhanced antimicrobial activity
    Rennukka M, Sipaut CS, Amirul AA
    Biotechnol Prog, 2014 Nov-Dec;30(6):1469-79.
    PMID: 25181613 DOI: 10.1002/btpr.1986
    This work aims to shed light in the fabrication of poly(3-hydroxybutyrate-co-44%-4-hydroxybutyrate)[P(3HB-co-44%4HB)]/chitosan-based silver nanocomposite material using different contents of silver nanoparticle (SNP); 1-9 wt%. Two approaches were applied in the fabrication; namely solvent casting and chemical crosslinking via glutaraldehyde (GA). A detailed characterization was conducted in order to yield information regarding the nanocomposite material. X-ray diffraction analysis exhibited the nature of the three components that exist in the nanocomposite films: P(3HB-co-4HB), chitosan, and SNP. In term of mechanical properties, tensile strength, and elongation at break were significantly improved up to 125% and 22%, respectively with the impregnation of the SNP. The melting temperature of the nanocomposite materials was increased whereas their thermal stability was slightly changed. Scanning electron microscopy images revealed that incorporation of 9 wt% of SNP caused agglomeration but the surface roughness of the material was significantly improved with the loading. Staphylococcus aureus and Escherichia coli were completely inhibited by the nanocomposite films with 7 and 9 wt% of SNP, respectively. On the other hand, degradation of the nanocomposite materials outweighed the degradation of the pure copolymer. These bioactive and biodegradable materials stand a good chance to serve the vast need of biomedical applications namely management and care of wound as wound dressing.
    Matched MeSH terms: Silver/metabolism*; Silver/pharmacology; Silver/chemistry
  6. Fulltext Fabrication and characterization of gelatin stabilized silver nanoparticles under UV-light
    Darroudi M, Ahmad MB, Zak AK, Zamiri R, Hakimi M
    Int J Mol Sci, 2011;12(9):6346-56.
    PMID: 22016663 DOI: 10.3390/ijms12096346
    Silver nanoparticles (Ag-NPs) were successfully synthesized using the UV irradiation of aqueous solutions containing AgNO(3) and gelatin as a silver source and stabilizer, respectively. The UV irradiation times influence the particles' diameter of the Ag-NPs, as evidenced from surface plasmon resonance (SPR) bands and transmission electron microscopy (TEM) images. When the UV irradiation time was increased, the mean size of particles continuously decreased as a result of photoinduced Ag-NPs fragmentation. Based on X-ray diffraction (XRD), the UV-irradiated Ag-NPs were a face-centered cubic (fcc) single crystal without any impurity. This study reveals that the UV irradiation-mediated method is a green chemistry and promising route for the synthesis of stable Ag-NPs for several applications (e.g., medical and surgical devices). The important advantages of this method are that it is cheap, easy, and free of toxic materials.
    Matched MeSH terms: Silver/chemistry*; Silver Nitrate/chemistry
  7. Polymeric structure of (ethylenediamine)silver(I) 3-nitrobenzoate monohydrate
    Usman A, Fun HK, Chantrapromma S, Zhu HL, Wang XJ
    Acta Crystallogr C, 2003 Mar;59(Pt 3):m97-9.
    PMID: 12711770
    In the ternary title compound, catena-poly[[silver(I)-mu-ethylenediamine-kappa(2)N:N'] 3-nitrobenzoate monohydrate], [[Ag(C(2)H(8)N(2))](C(7)H(4)NO(4)) x H(2)O](n), the Ag atom is bicoordinated in a linear configuration by two different N atoms from two symmetry-related ethylenediamine ligands, thus giving linear polymeric chains with an [-Ag-N-C-C-N-](n) backbone running parallel to the a axis. In the crystal packing, these linear chains are interconnected by N-H...O and O-H...O hydrogen bonds to form layers parallel to the ab plane.
    Matched MeSH terms: Silver
  8. Studies on Echinostomatidae (Trematoda) in Malaya. 13. Integumentary papillae on six species of Echinostome cercariae
    Lie KJ
    J Parasitol, 1966 Dec;52(6):1041-8.
    PMID: 4162735
    Matched MeSH terms: Silver Nitrate
  9. Fulltext Synergistic enhancement in the microelectronic properties of poly-(dioctylfluorene) based Schottky devices by CdSe quantum dots
    Muhammad F, Tahir M, Zeb M, Kalasad MN, Mohd Said S, Sarker MR, et al.
    Sci Rep, 2020 Mar 16;10(1):4828.
    PMID: 32179797 DOI: 10.1038/s41598-020-61602-1
    This paper reports the potential application of cadmium selenide (CdSe) quantum dots (QDs) in improving the microelectronic characteristics of Schottky barrier diode (SBD) prepared from a semiconducting material poly-(9,9-dioctylfluorene) (F8). Two SBDs, Ag/F8/P3HT/ITO and Ag/F8-CdSe QDs/P3HT/ITO, are fabricated by spin coating a 10 wt% solution of F8 in chloroform and 10:1 wt% solution of F8:CdSe QDs, respectively, on a pre-deposited poly(3-hexylthiophene) (P3HT) on indium tin oxide (ITO) substrate. To study the electronic properties of the fabricated devices, current-voltage (I-V) measurements are carried out at 25 °C in dark conditions. The I-V curves of Ag/F8/P3HT/ITO and Ag/F8-CdSe QDs/P3HT/ITO SBDs demonstrate asymmetrical behavior with forward bias current rectification ratio (RR) of 7.42 ± 0.02 and 142 ± 0.02, respectively, at ± 3.5 V which confirm the formation of depletion region. Other key parameters which govern microelectronic properties of the fabricated devices such as charge carrier mobility (µ), barrier height (ϕb), series resistance (Rs) and quality factor (n) are extracted from their corresponding I-V characteristics. Norde's and Cheung functions are also applied to characterize the devices to study consistency in various parameters. Significant improvement is found in the values of Rs, n, and RR by 3, 1.7, and 19 times, respectively, for Ag/F8-CdSe QDs/P3HT/ITO SBD as compared to Ag/F8/P3HT/ITO. This enhancement is due to the incorporation of CdSe QDs having 3-dimensional quantum confinement and large surface-to-volume area. Poole-Frenkle and Richardson-Schottky conduction mechanisms are also discussed for both of the devices. Morphology, optical bandgap (1.88 ± 0.5 eV) and photoluminescence (PL) spectrum of CdSe QDs with a peak intensity at 556 nm are also reported and discussed.
    Matched MeSH terms: Silver
  10. Single-step green route synthesis of Au/Ag bimetallic nanoparticles using clove buds extract: Enhancement in antioxidant bio-efficacy and catalytic activity
    Sharma C, Ansari S, Ansari MS, Satsangee SP, Srivastava MM
    Mater Sci Eng C Mater Biol Appl, 2020 Nov;116:111153.
    PMID: 32806256 DOI: 10.1016/j.msec.2020.111153
    In present work, we demonstrate a single step environmentally benign approach to synthesize Au/Ag bimetallic nanoparticles (BMNPs) using aqueous extract of Clove buds for the first time. Clove bud's (CB) extract has proficiency to act as a reducing and stabilizing agent for the formation of Au/Ag BMNPs. In presence of extract, AuIII and AgI are reduced competitively within same solution and produce Au/Ag alloy NPs. The kinetics besides the formation of NPs was studied using UV-visible spectroscopy and efficiency of the extract was monitored by varying contact time, temperature, pH and extract concentration. The electron microscopic studies revealed the presence of NPs with peculiar morphology at alkaline pH. Further, the existence of Au and Ag atoms was investigated using energy dispersive X-ray (EDX), X-ray diffraction (XRD) and cyclic voltammetry (CV) techniques. Fourier transform infrared spectroscopy (FTIR) showed that Eugenol in the extract is mainly responsible for the production of NPs which are also surrounded by various phytochemicals. Zeta potential of all the NPs is found to be negative which prevents their agglomeration due to inter-repulsion and the biosynthesized Au/Ag BMNPs revealed greater catalytic efficiency for the degradation of methyl orange (MO), methylene blue (MB) and reduction of p-nitrophenol (p-NP). Significant enhancement induced by BMNPs compared to individual monometallic nanoparticles (MMNPs) was assigned to the synergistic effect of MMNPs and coating of phytochemicals present in the CB extract.
    Matched MeSH terms: Silver
  11. Indole Synthesis Using Silver Catalysis
    Clarke AK, Ho HE, Rossi-Ashton JA, Taylor RJK, Unsworth WP
    Chem Asian J, 2019 Mar 25.
    PMID: 30908897 DOI: 10.1002/asia.201900309
    Indoles are amongst the most important class of heteroaromatics in organic chemistry, being commonly found in biologically active natural products and therapeutically useful compounds. The synthesis of indoles is therefore important and several methods for their synthesis that make use of silver(I) catalysts and reagents have been developed in recent years. This Focus Review contains, to the best of our knowledge, a comprehensive coverage of silver-mediated indole forming reactions since the first reaction of this type was reported in 2004.
    Matched MeSH terms: Silver
  12. Fulltext Crystal structure of benzyl-tri-phenyl-phospho-nium chloride monohydrate
    Ahmad J, Abdul Halim SN, How FN
    Acta Crystallogr E Crystallogr Commun, 2015 Jun 1;71(Pt 6):o410-1.
    PMID: 26090195 DOI: 10.1107/S2056989015009159
    The title compound, Ph3(PhCH2)P(+)·Cl(-)·H2O, was obtained unintentionally as the product of an attempted synthesis of a silver di-thio-carbamate complex using benzyl-tri-phenyl-phospho-nium as the counter-ion. The asymmetric unit consists of a phospho-nium cation and a chloride anion, and a water mol-ecule of crystallization. In the crystal, the chloride ion is linked to the water mol-ecule by an O-H⋯Cl hydrogen bond. The three units are further linked via C-H⋯Cl and C-H⋯O hydrogen bonds and C-H⋯ π inter-actions, forming a three-dimensional structure.
    Matched MeSH terms: Silver
  13. Fulltext Thickness Optimization of Thin-Film Tandem Organic Solar Cell
    Bangash KA, Kazmi SAA, Farooq W, Ayub S, Musarat MA, Alaloul WS, et al.
    Micromachines (Basel), 2021 May 05;12(5).
    PMID: 34062988 DOI: 10.3390/mi12050518
    The polymer solar cells also known as organic solar cells (OSCs) have drawn attention due to their cynosure in industrial manufacturing because of their promising properties such as low weight, highly flexible, and low-cost production. However, low η restricts the utilization of OSCs for potential applications such as low-cost energy harvesting devices. In this paper, OSCs structure based on a triple-junction tandem scheme is reported with three different absorber materials to enhance the absorption of photons which in turn improves the η, as well as its correlating performance parameters. The investigated structure gives the higher value of η = 14.33% with Jsc = 16.87 (mA/m2), Voc = 1.0 (V), and FF = 84.97% by utilizing a stack of three different absorber layers with different band energies. The proposed structure was tested under 1.5 (AM) with 1 sun (W/m2). The impact of the top, middle, and bottom subcells' thickness on η was analyzed with a terse to find the optimum thickness for three subcells to extract high η. The optimized structure was then tested with different electrode combinations, and the highest η was recorded with FTO/Ag. Moreover, the effect of upsurge temperature was also demonstrated on the investigated schematic, and it was observed that the upsurge temperature affects the photovoltaic (PV) parameters of the optimized cell and η decreases from 14.33% to 11.40% when the temperature of the device rises from 300 to 400 K.
    Matched MeSH terms: Silver
  14. Carrier-Gas Induced Changes in the Structural, Stoichiometric and Photocatalytic Characteristics of Gallium Oxide Nanostructures
    Jubu PR, Yam FK
    J Nanosci Nanotechnol, 2021 Oct 01;21(10):5266-5274.
    PMID: 33875117 DOI: 10.1166/jnn.2021.19456
    Ga₂O₃/ITO/glass photoelectrodes prepared by the CVD method has rarely been tested in the electrochemical cell for water splitting. In this study, we investigate the photoelectrolytic performance of Ga₂O₃/ITO-glass photocatalysts produced by the high-temperature CVD route. The changing of N₂ carrier gas flow rate from 0 to 1800 seem induces change in the materials properties. XRD signal strength of the produced bi-phase Ga₂O₃ is observed to deteriorate, while diffraction line width broadens with increasing N₂ supply. Films show a combination of nanoclumps and nanostrips morphology. Ga/O ratio decreases, while the optical bandgap gradually increases from 4.37 to 4.42 eV with increasing O content and crystallite size. Photoluminescence measurements show UV, blue, green and red emissions, respectively. Linear sweep voltammetry of the electrodes in 0.1 M KOH electrolyte shows improvement in photocurrent density from 160 to 257 μA/cm² versus Ag/AgCl at 1 V bias, and a maximum photon-to-current conversion efficiency 0.06%.
    Matched MeSH terms: Silver
  15. Fulltext Physical properties of single jersey bamboo cotton fabric produced on home knitting machine
    Ainil Huda Abu Talib, Siti Nuranis Syazana Misron, Nurul ‘izzah Mohd Fu’ad, Nurul Ariesha Zamri, Eryna Nasir
    Borneo Akademika, 2020;4(1):13-24.
    MyJurnal
    The Silver Reed Model LK150 knitting machine is a home knitting machine which is
    extremely lightweight and compact, making it preferable by most home knitters.
    There are various knitwears with interesting patterns can be made using this model. In
    the field of garments manufacturing by using flatbed knitting machines, it is
    important to understand the physical properties of fabric so that their impact on
    dimensional changes can be predicted to produce the most suitable end use. The
    samples were produced by using a blended bamboo/cotton yarn, with a composition
    of 30% cotton and 70% bamboo. The main objectives of this study are to to evaluate
    the physical properties of single jersey fabric knitted on home knitting machine by
    using different stitch dials and to relate the physical properties with different stitch
    lengths. Then, all tests were conducted to compare the physical properties of samples
    between three different stitch dials and the effects of before and after washing. The
    physical properties measured in this research were stitch length, stitch density, weight,
    thickness, absorbency and shrinkage. The result indicated that the longer the stitch
    length, the higher the percentage of the water impact penetration. Meanwhile, there
    was a slight reduction on the density, thickness and fabric weight. In addition, the
    result after three times washing showed that the samples only had slight changes in
    density, thickness, weight and stitch length, but has significant changes on the water
    impact penetration.
    Matched MeSH terms: Silver
  16. Fulltext The effects of Carica papaya Linn. latex on the healing of burn wounds in rats
    Ahmad Nazrun Shuid, Mohd Syukri Anwar, Ahmad Asmadi Yusof
    Jurnal Sains Kesihatan Malaysia, 2005;3(2):39-47.
    MyJurnal
    This study was carried out to compare the rate of burn wound healing with the applications of the latex of Carica papaya Linn. (papaya) or of silver sulfadiazine cream (SSD). Partial and full thickness burn wound (2 cm x 2 cm) was induced on the dorsal part of anaesthetized rats by using heated metal plates. The rats were divided into three groups, i.e. untreated group and groups treated daily with SSD and papaya latex, respectively. A digital camera was used to take photographs of the burn wounds daily to monitor their healing. It was found that there was no significant difference in the healing time of papaya latex treated group compared to the SSD treated group. Papaya latex contained digestive enzymes which might clean burn wounds but might also cause wound bleeding in a few rats of the papaya latex group.
    Matched MeSH terms: Silver Sulfadiazine
  17. Pleurotus sajor-caju can be used to synthesize silver nanoparticles with antifungal activity against Candida albicans
    Musa SF, Yeat TS, Kamal LZM, Tabana YM, Ahmed MA, El Ouweini A, et al.
    J Sci Food Agric, 2018 Feb;98(3):1197-1207.
    PMID: 28746729 DOI: 10.1002/jsfa.8573
    BACKGROUND: Green synthesis of silver nanoparticles (AgNPs) has become widely practiced worldwide. In this study, AgNPs were synthesized using a hot-water extract of the edible mushroom Pleurotus sajor-caju. The product, PSC-AgNPs, was characterized by using UV-visible spectra, dynamic light scattering analysis, transmission electron microscopy (TEM), X-ray diffraction (XRD) and Fourier transform infrared (FTIR) spectrometry. To assess its antifungal activity against Candida albicans, gene transcription and protein expression analyses were conducted for CaICL1 and its product, ICL, using real-time quantitative polymerase chain reaction and western blot, respectively.

    RESULTS: PSC-AgNPs with an average particle size of 11.68 nm inhibited the growth of the pathogenic yeast C. albicans. Values for minimum inhibitory concentration and minimum fungicidal concentration were 250 and 500 mg L-1 , respectively. TEM images revealed that the average particle size of PSC-AgNPs was 16.8 nm, with the values for zeta potential and the polydispersity index being -8.54 mV and 0.137, respectively. XRD and FTIR spectra showed PSC-AgNPs to have a face-centered cubic crystalline structure. The polysaccharides and amino acid residues present in P. sajor-caju extract were found to be involved in reducing Ag+ to AgNP. Both CaICL1 transcription and ICL protein expression were found to be suppressed in the cells treated with PSC-AgNPs as compared with the control.

    CONCLUSION: Our PSC-AgNP preparation makes for a promising antifungal agent that can downregulate isocitrate lyase. © 2017 Society of Chemical Industry.

    Matched MeSH terms: Silver/metabolism*; Silver/pharmacology*; Silver/chemistry
  18. Frequency, size and location of apical and lateral foramina in anterior permanent teeth
    Abdullah D, Kanagasingam S, Luke D
    Sains Malaysiana, 2013;42:81-84.
    The aim of the study was to determine the frequency, size and location of apical and lateral foramina on anterior teeth. A total of 100 anterior teeth consisting of maxillary and mandibular incisors and canines were fixed in 10% formalin. Periodontal tissue remnants were mechanically removed and teeth were stained in 2% aqueous silver nitrate. The teeth were dried and examined using a Leica MZ 7.5 zoom stereomicroscope. The size of apical and lateral foramina and their distance from the anatomical apex of the tooth were measured directly using a calibrated eyepiece scale. Accessory foramina more than 1.8 mm from the apex were regarded as lateral foramina. Eighteen percent of teeth possessed more than one apical foramen. Seven teeth (three maxillary centrals, three maxillary canines, one mandibular lateral) had 11 lateral foramina each. The mean diameter of the lateral foramina was 0.14 mm (SD = 0.08) and their mean distance from the apex was 4.49 mm (SD = 2.63, range 1.9-10.5 mm). Multiple foramina were most common on maxillary canines and least common on maxillary laterals. The mean diameter of apical foramina for all teeth possessing a single foramen was 0.35 mm (SD = 0.10) and the mean apical foramen diameter for all teeth with multiple apical foramina was 0.22 mm (SD = 0.08). Most anterior teeth possess one apical foramen and no lateral foramina; about 20% possessed more than one apical foramen and about 10% possessed one or more lateral foramina. These findings should be considered when root-treating anterior teeth.
    Matched MeSH terms: Silver Nitrate
  19. L-cysteine capped silver nanoparticles as chiral recognition sensor for ketoprofen enantiomers
    Obaid A, Mohd Jamil AK, Saharin SM, Mohamad S
    Chirality, 2021 11;33(11):810-823.
    PMID: 34486177 DOI: 10.1002/chir.23354
    A simple, inexpensive but effective approach for visual chiral recognition of ketoprofen enantiomers was developed using L-cysteine capped silver nanoparticles (L-Cys-AgNPs) as a colorimetric sensor. Upon the addition of R-ketoprofen to L-Cys-AgNPs, rapid aggregation occurred, and the solution changed color from yellow to green. However, the presence of S-ketoprofen did not induce any color change. The results were characterized using UV-Vis, FESEM, FT-IR, SERS, and zeta potential measurements. The chiral assay described in this work is easily distinguished with the naked eyes or using a UV-Vis spectrometer. The sensor revealed a good linear response to ketoprofen enantiomers in the concentration range of 8.33-33.3 μM with a detection limit of 4.52 μM and relative standard deviation of 3.73%. The proposed method was utilized for the determination of ketoprofen racemic mixtures in water samples and commercial tablets. The method excels by its simplicity, low cost, and good availability of materials.
    Matched MeSH terms: Silver
  20. Anti-plasmodial activity of aqueous neem leaf extract mediated green synthesis-based silver nitrate nanoparticles
    Ghazali SZ, Mohamed Noor NR, Mustaffa KMF
    Prep Biochem Biotechnol, 2022;52(1):99-107.
    PMID: 33890844 DOI: 10.1080/10826068.2021.1913602
    The objective of this study is to synthesize neem-silver nitrate nanoparticles (neem-AgNPs) using aqueous extracts of Azadirachta indica A. Juss for malaria therapy. Neem leaves collected from FRIM Malaysia were authenticated and extracted using Soxhlet extraction method. The extract was introduced to 1 mM of silver nitrate solution for neem-AgNPs synthesis. Synthesized AgNPs were further characterized by ultraviolet-visible spectroscopy and the electron-scanning microscopy. Meanwhile, for the anti-plasmodial activity of the neem-AgNPs, two lab-adapted Plasmodium falciparum strains, 3D7 (chloroquine-sensitive), and W2 (chloroquine-resistant) were tested. Red blood cells hemolysis was monitored to observe the effects of neem-AgNPs on normal and parasitized red blood cells. The synthesized neem-AgNPs were spherical in shape and showed a diameter range from 31-43 nm. When compared to aqueous neem leaves extract, the half inhibitory concentration (IC50) of the synthesized neem-AgNPs showed a four-fold IC50 decrease against both parasite strains with IC50 value of 40.920 µg/mL to 8.815 µg/mL for 3D7, and IC50 value of 98.770 µg/mL to 23.110 µg/mL on W2 strain. The hemolysis assay indicates that the synthesized neem-AgNPs and aqueous extract alone do not have hemolysis activity against normal and parasitized red blood cells. Therefore, this study shows the synthesized neem-AgNPs has a great potential to be used for malaria therapy.
    Matched MeSH terms: Silver Nitrate/chemical synthesis; Silver Nitrate/pharmacology; Silver Nitrate/chemistry*
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