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  1. Zukerman-Schpector J, Maganhi SH, Moran PJ, de Paula BR, Nucci PR, Tiekink ER
    Acta Crystallogr Sect E Struct Rep Online, 2014 Sep 1;70(Pt 9):o1020-1.
    PMID: 25309202 DOI: 10.1107/S1600536814018327
    In the title compound, C17H15NO4, the conformation about the C=C double bond [1.348 (2) Å] is E with the ketone group almost co-planar [C-C-C-C torsion angle = 7.2 (2)°] but the phenyl group twisted away [C-C-C-C = 160.93 (17)°]. The terminal aromatic rings are almost perpendicular to each other [dihedral angle = 81.61 (9)°] giving the mol-ecule an overall U-shape. The crystal packing feature benzene-C-H⋯O(ketone) contacts that lead to supra-molecular helical chains along the b axis. These are connected by π-π inter-actions between benzene and phenyl rings [inter-centroid distance = 3.6648 (14) Å], resulting in the formation of a supra-molecular layer in the bc plane.
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