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Abstract:
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  1. Al-Mehana WN, Yahya R, Lo KM
    PMID: 22219934 DOI: 10.1107/S160053681104102X
    The mol-ecule of the title compound, C(20)H(16)N(2)O(2), is centrosymmetric with the mid-point of the central N-N bond located on an inversion center. The configuration around the C=N bond is E. The whole mol-ecule (except for the H atoms) is approximately planar, with an r.m.s. deviation of 0.07 Å. In the crystal, the presence of weak inter-molecular C-H⋯O hydrogen bonding involving each acetyl-ene H atom and the adjacent phen-oxy O atom results in the formation of supra-molecular chains.
  2. Al-Mehana WN, Yahya R, Sonsudin F, Al-Mehana IN, Lo KM
    Acta Crystallogr Sect E Struct Rep Online, 2012 Oct 1;68(Pt 10):o2990.
    PMID: 23125764 DOI: 10.1107/S1600536812038354
    The complete molecule of the title compound, C(18)H(20)N(2)O(4), is generated by inversion symmetry. The conformation around the C=N bond is E. With the exception of the eth-oxy substituent, the mol-ecule is essentially planar with an r.m.s. deviation of 0.0455 Å. In the crystal, mol-ecules are linked by O-H⋯N hydrogen bonds into a two-dimensional supra-molecular network parallel to the bc plane.
  3. Al-Mehana WN, Shakir RM, Yahya R, Abd Halim SN, Tiekink ER
    Acta Crystallogr Sect E Struct Rep Online, 2011 Jul 1;67(Pt 7):o1659.
    PMID: 21837059 DOI: 10.1107/S1600536811022410
    The complete mol-ecule in the title compound, C(22)H(20)N(2)O(4), is generated by the application of an inversion centre. With the exception of the terminal acetyl-ene groups [C-O-C-C = -78.02 (17)°], the remaining atoms constituting the mol-ecule are essentially coplanar. The configuration around the C=N bond [1.282 (2) Å] is E. The formation of supra-molecular chains mediated by C-H⋯O inter-actions, occurring between methyl-ene H and meth-oxy O atoms, is the most notable feature of the crystal packing.
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