The effect of chamber pressure of a freeze dryer on essential oil contents, drying kinetics, drying characteristics lemon balm leaves and morphology of lemon balm glandular trichomes (oil reservoirs) were investigated. It was found that overall freeze drying (FD) carried out at high (FD-HP) and low pressure (FD-LP) settings consist of sublimation rate, first falling rate and second falling rate periods. Drying rate of FD-LP dried Lemon Balm leaves are higher than FD-HP dried samples, where the drying rates ranged from 0.063 to 0.449 g H2O/ g DM. s and 0.0365 to 0.395 g H2O/ g DM. s, respectively. 3rd order Polynomial model was found to be the best fit model for both drying kinetics. In terms of product quality, eight (8) major constituents of lemon balm leaves essential oil were quantified. Further to this, electro-microscope was used to observe the peltate glandular hairs structure. Product quality analysis showed that FD-HP retained higher amount of essential oil, shape of glandular hairs, but no positive effect on the freeze drying duration.
The drying of Piper betle Linn (betel) leaf extract using a lab scale spray dryer was simulated using Computational Fluid Dynamics (CFD). Three different turbulent models (standard k-ε, RNG k-ε and realizable k-ε) were used in the present study to determine the most suitable model for predicting the flow profile. Parametric studies were also conducted to evaluate the effect of process variables on the final moisture content. Four different initial droplet sizes (36, 79, 123 and 166 μm) were tested with four sets of combination of hot air temperature (140 and 160°C) and feed rate (4, 9.5 and 15 ml/min). It was found that standard k-ε is the most suitable turbulent model to predict the flow behaviour Moreover, the lowest final moisture content present in samples was obtained at 140°C and a feed rate of 15.0 ml/min.