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  1. Caracelli I, Maganhi SH, Stefani HA, Gueogjian K, Tiekink ER
    Acta Crystallogr E Crystallogr Commun, 2015 Feb 1;71(Pt 2):o90-1.
    PMID: 25878887 DOI: 10.1107/S2056989014027790
    The coumarin ring system in the title asymmetric alkyne, C18H12O2, is approximately planar (r.m.s. deviation of the 11 non-H atoms = 0.048 Å), and is inclined with respect to the methyl-benzene ring, forming a dihedral angle of 33.68 (4)°. In the crystal, supra-molecular zigzag chains along the c-axis direction are formed via weak C-H⋯O hydrogen bonds, and these are connected into double layers via weak C-H⋯π inter-actions; these stack along the a axis.
  2. Caracelli I, Maganhi SH, Stefani HA, Gueogjian K, Tiekink ER
    Acta Crystallogr E Crystallogr Commun, 2015 Mar 01;71(Pt 3):o154-5.
    PMID: 25844223 DOI: 10.1107/S2056989015002157
    In the title compound, C15H8O2S, the coumarin moiety is approximately planar (r.m.s. deviation of the 11 non-H atoms = 0.025 Å) and is slightly inclined with respect to the plane of the thio-phen-3-yl ring, forming a dihedral angle of 11.75 (8)°. In the crystal, the three-dimensional architecture features a combination of coumarin-thio-phene C-H⋯π and π-π [inter-centroid distance = 3.6612 (12) Å] inter-actions.
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