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Fulltext Crystal structure of ethyl 2-[(4-bromo-phen-yl)amino]-3,4-di-methyl-pent-3-enoate

Zukerman-Schpector J, Caracelli I, Stefani HA, Khan AN, Tiekink ER

Acta Crystallogr Sect E Struct Rep Online, 2014 Oct 1;70(Pt 10):o1122-3.
PMID: 25484707 DOI: 10.1107/S1600536814020832

In the title compound, C15H20BrNO2, there are two independent mol-ecules (A and B) comprising the asymmetric unit and these adopt very similar conformations. In A, the dihedral angle between the CO2 and MeC=CMe2 groups is 80.7 (3)°, and these make dihedral angles of 3.5 (3) and 84.09 (16)°, respectively, with the bromo-benzene ring. The equivalent dihedral angles for mol-ecule B are 78.4 (3), 2.1 (3) and 78.37 (12)°, respectively. The most prominent inter-actions in the crystal packing are amine-N-H⋯O(carbon-yl) hydrogen bonds between the two independent mol-ecules, resulting in non-centrosymmetric ten-membered {⋯OC2NH}2 synthons. Statistical disorder is noted for each of the terminal methyl groups of the ethyl residues.
Fulltext Energy-efficient routing protocol for reliable low-latency Internet of Things in oil and gas pipeline monitoring

Karam SN, Bilal K, Khan AN, Shuja J, Abdulkadir SJ

PeerJ Comput Sci, 2024;10:e1908.
PMID: 38435610 DOI: 10.7717/peerj-cs.1908

The oil and gas industries (OGI) are the primary global energy source, with pipelines as vital components for OGI transportation. However, pipeline leaks pose significant risks, including fires, injuries, environmental harm, and property damage. Therefore, maintaining an effective pipeline maintenance system is critical for ensuring a safe and sustainable energy supply. The Internet of Things (IoT) has emerged as a cutting-edge technology for efficient OGI pipeline leak detection. However, deploying IoT in OGI monitoring faces significant challenges due to hazardous environments and limited communication infrastructure. Energy efficiency and fault tolerance, typical IoT concerns, gain heightened importance in the OGI context. In OGI monitoring, IoT devices are linearly deployed with no alternative communication mechanism available along OGI pipelines. Thus, the absence of both communication routes can disrupt crucial data transmission. Therefore, ensuring energy-efficient and fault-tolerant communication for OGI data is paramount. Critical data needs to reach the control center on time for faster actions to avoid loss. Low latency communication for critical data is another challenge of the OGI monitoring environment. Moreover, IoT devices gather a plethora of OGI parameter data including redundant values that hold no relevance for transmission to the control center. Thus, optimizing data transmission is essential to conserve energy in OGI monitoring. This article presents the Priority-Based, Energy-Efficient, and Optimal Data Routing Protocol (PO-IMRP) to tackle these challenges. The energy model and congestion control mechanism optimize data packets for an energy-efficient and congestion-free network. In PO-IMRP, nodes are aware of their energy status and communicate node's depletion status timely for network robustness. Priority-based routing selects low-latency routes for critical data to avoid OGI losses. Comparative analysis against linear LEACH highlights PO-IMRP's superior performance in terms of total packet transmission by completing fewer rounds with more packet's transmissions, attributed to the packet optimization technique implemented at each hop, which helps mitigate network congestion. MATLAB simulations affirm the effectiveness of the protocol in terms of energy efficiency, fault-tolerance, and low latency communication.
Fulltext Practice nurses and pharmacists: a perspective on the expectation and experience of nurses for future collaboration

Khan AN, Khan MU, Shoaib MH, Yousuf RI, Mir SA

Oman Med J, 2014 Jul;29(4):271-5.
PMID: 25170408 DOI: 10.5001/omj.2014.71

OBJECTIVES: To explore the nurses' expectations and experience about pharmacists in private sector hospitals of Karachi, Pakistan.
METHODS: A cross-sectional study was conducted from June to September 2012 in five private sector hospitals of Karachi, Pakistan. A convenient sample of nurses (n=377) were enrolled in this study. Data was obtained through a previously validated questionnaire. Responses were statistically analyzed using SPSSv.17.
RESULTS: Questionnaires were returned giving a response rate of 63.6% of which 20 were unusable (n=240). Out of the remaining 220, 24.1% (n=53) responded that they never or rarely interacted with a pharmacist. Respondents who expect pharmacists to collaborate with nurses to solve drug related problems were 45% (n=99). Nurses' experience of pharmacists was not substantial as only 44.5% (n=98) respondents consider pharmacists as a reliable source of clinical drug information.
CONCLUSION: The role of pharmacists is not well appreciated among nurses in Pakistan. Hence, pharmacists must bridge the observed gap and use a more strategic and consistent approach to build a more positive image in line with other healthcare professionals and in providing patient-centred pharmaceutical care. This research would impress upon the pharmacists the need to redefine their role in the healthcare settings.

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