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Fulltext Numerical Prediction of Residual Stresses Distribution in Thin-Walled Press-Braked Stainless Steel Sections

Mutafi A, Yidris N, Koloor SSR, Petrů M

Materials (Basel), 2020 Nov 26;13(23).
PMID: 33256257 DOI: 10.3390/ma13235378

Stainless steels are increasingly used in construction today, especially in harsh environments, in which steel corrosion commonly occurs. Cold-formed stainless steel structures are currently increasing in popularity because of its efficiency in load-bearing capacity and its appealing architectural appearance. Cold-rolling and press-braking are the cold-working processes used in the forming of stainless steel sections. Press braking can produce large cross-sections from thin to thick-walled sections compared to cold-rolling. Cold-forming in press-braked sections significantly affect member behaviour and joints; therefore, they have attained great attention from many researchers to initiate investigations on those effects. This paper examines the behaviour of residual stress distribution of stainless steel press-braked sections by implementing three-dimensional finite element (3D-FE) technique. The study proposed a full finite element procedure to predict the residual stresses starting from coiling-uncoiling to press-braking. This work considered material anisotropy to examine its effect on the residual stress distribution. The technique adopted was compared with different finite element techniques in the literature. This study also provided a parametric study for three corner radius-to-thickness ratios looking at the through-thickness residual stress distribution of four stainless steels (i.e., ferritic, austenitic, duplex, lean duplex) in which have their own chemical composition. In conclusion, the comparison showed that the adopted technique provides a detailed prediction of residual stress distribution. The influence of geometrical aspects is more pronounced than the material properties. Neglecting the material anisotropy shows higher shifting in the neutral axis. The parametric study showed that all stainless steel types have the same stress through-thickness distribution. Moreover, R/t ratios' effect is insignificant in all transverse residual stress distributions, but a slight change to R/t ratios can affect the longitudinal residual stress distribution.
Fulltext Separation of ctDNA by superparamagnetic bead particles in microfluidic platform for early cancer detection

Balakrishnan SG, Ahmad MR, Koloor SSR, Petrů M

J Adv Res, 2021 Nov;33:109-116.
PMID: 34603782 DOI: 10.1016/j.jare.2021.03.001

INTRODUCTION: Conventional biopsy, based on extraction from a tumor of a solid tissue specimen requiring needles, endoscopic devices, excision or surgery, is at risk of infection, internal bleeding or prolonged recovery. A non-invasive liquid biopsy is one of the greatest axiomatic consequences of the identification of circulating tumor DNA (ctDNA) as a replaceable surgical tumor bioQpsy technique. Most of the literature studies thus far presented ctDNA detection at almost final stage III or IV of cancer, where the treatment option or cancer management is nearly impossible for diagnosis.
OBJECTIVE: Hence, this paper aims to present a simulation study of extraction and separation of ctDNA from the blood plasma of cancer patients of stage I and II by superparamagnetic (SPM) bead particles in a microfluidic platform for early and effective cancer detection.
METHOD: The extraction of ctDNA is based on microfiltration of particle size to filter some impurities and thrombocytes plasma, while the separation of ctDNA is based on magnetic manipulation to high yield that can be used for the upstream process.
RESULT: Based on the simulation results, an average of 5.7 ng of ctDNA was separated efficiently for every 10 µL blood plasma input and this can be used for early analysis of cancer management. The particle tracing module from COMSOL Multiphysics traced ctDNA with 65.57% of sensitivity and 95.38% of specificity.
CONCLUSION: The findings demonstrate the ease of use and versatility of a microfluidics platform and SPM bead particles in clinical research related to the preparation of biological samples. As a sample preparation stage for early analysis and cancer diagnosis, the extraction and separation of ctDNA is most important, so precision medicine can be administered.
Fulltext Moisture Absorption Effects on Mode II Delamination of Carbon/Epoxy Composites

Wong KJ, Johar M, Koloor SSR, Petrů M, Tamin MN

Polymers (Basel), 2020 Sep 22;12(9).
PMID: 32971855 DOI: 10.3390/polym12092162

It is necessary to consider the influence of moisture damage on the interlaminar fracture toughness for composite structures that are used for outdoor applications. However, the studies on the progressive variation of the fracture toughness as a function of moisture content M (%) is rather limited. In this regard, this study focuses on the characterization of mode II delamination of carbon/epoxy composites conditioned at 70 °C/85% relative humidity (RH). End-notched flexure test is conducted for specimens aged at various moisture absorption levels. Experimental results reveal that mode II fracture toughness degrades with the moisture content, with a maximum of 23% decrement. A residual property model is used to predict the variation of the fracture toughness with the moisture content. Through numerical simulations, it is found that the approaches used to estimate the lamina and cohesive properties are suitable to obtain reliable simulation results. In addition, the damage initiation is noticed during the early loading stage; however, the complete damage is only observed when the numerical peak load is achieved. Results from the present research could serve as guidelines to predict the residual properties and simulate the mode II delamination behavior under moisture attack.
Fulltext Nano-Level Damage Characterization of Graphene/Polymer Cohesive Interface under Tensile Separation

Koloor SSR, Rahimian-Koloor SM, Karimzadeh A, Hamdi M, Petrů M, Tamin MN

Polymers (Basel), 2019 Sep 02;11(9).
PMID: 31480660 DOI: 10.3390/polym11091435

The mechanical behavior of graphene/polymer interfaces in the graphene-reinforced epoxy nanocomposite is one of the factors that dictates the deformation and damage response of the nanocomposites. In this study, hybrid molecular dynamic (MD) and finite element (FE) simulations of a graphene/polymer nanocomposite are developed to characterize the elastic-damage behavior of graphene/polymer interfaces under a tensile separation condition. The MD results show that the graphene/epoxy interface behaves in the form of elastic-softening exponential regressive law. The FE results verify the adequacy of the cohesive zone model in accurate prediction of the interface damage behavior. The graphene/epoxy cohesive interface is characterized by normal stiffness, tensile strength, and fracture energy of 5 × 10-8 (aPa·nm-1), 9.75 × 10-10 (nm), 2.1 × 10-10 (N·nm-1) respectively, that is followed by an exponential regressive law with the exponent, α = 7.74. It is shown that the commonly assumed bilinear softening law of the cohesive interface could lead up to 55% error in the predicted separation of the interface.
Fulltext Thermal Delamination Modelling and Evaluation of Aluminium-Glass Fibre-Reinforced Polymer Hybrid

Chow ZP, Ahmad Z, Wong KJ, Koloor SSR, Petrů M

Polymers (Basel), 2021 Feb 04;13(4).
PMID: 33557350 DOI: 10.3390/polym13040492

This paper aims to propose a temperature-dependent cohesive model to predict the delamination of dissimilar metal-composite material hybrid under Mode-I and Mode-II delamination. Commercial nonlinear finite element (FE) code LS-DYNA was used to simulate the material and cohesive model of hybrid aluminium-glass fibre-reinforced polymer (GFRP) laminate. For an accurate representation of the Mode-I and Mode-II delamination between aluminium and GFRP laminates, cohesive zone modelling with bilinear traction separation law was implemented. Cohesive zone properties at different temperatures were obtained by applying trends of experimental results from double cantilever beam and end notched flexural tests. Results from experimental tests were compared with simulation results at 30, 70 and 110 °C to verify the validity of the model. Mode-I and Mode-II FE models compared to experimental tests show a good correlation of 5.73% and 7.26% discrepancy, respectively. Crack front stress distribution at 30 °C is characterised by a smooth gradual decrease in Mode-I stress from the centre to the edge of the specimen. At 70 °C, the entire crack front reaches the maximum Mode-I stress with the exception of much lower stress build-up at the specimen's edge. On the other hand, the Mode-II stress increases progressively from the centre to the edge at 30 °C. At 70 °C, uniform low stress is built up along the crack front with the exception of significantly higher stress concentrated only at the free edge. At 110 °C, the stress distribution for both modes transforms back to the similar profile, as observed in the 30 °C case.
Fulltext An Extended Thickness-Dependent Moisture Absorption Model for Unidirectional Carbon/Epoxy Composites

Azizan A, Johar M, Karam Singh SS, Abdullah S, Koloor SSR, Petrů M, et al.

Polymers (Basel), 2021 Jan 30;13(3).
PMID: 33573112 DOI: 10.3390/polym13030440

Moisture absorption tests for materials that exhibit non-Fickian behavior generally require a relatively long period to reach saturation. Therefore, it would be beneficial to establish a relationship between the moisture content and the thickness to minimize the experimental time and cost. This research characterizes the moisture absorption behavior of AS4/8552 carbon/epoxy composites. Specimens were prepared at 4, 8, and 16 plies and immersed in distilled water at 60 °C. The relationship between the non-Fickian parameters (Fickian to non-Fickian maximum moisture content ratio ϕ, non-Fickian diffusivity per square thickness α, and non-Fickian initiation time to) and thickness was characterized using a thickness-dependent model. A comparison with other materials revealed that all three non-Fickian parameters are able to be fitted using a power law. Nevertheless, the upper boundary for the applicability of this model was not determined in this study. The Weibull distribution plots indicate that the probability of non-Fickian moisture absorption is influenced by ϕ and α at approximately 62% within a normalized thickness range of 2-3. In regards to to, it is 82% at a normalized thickness of 6. Therefore, the Weibull distribution is proposed for the assessment of non-Fickian moisture absorption based on the material's thickness.