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  1. Rajendran Royan NR, Leong JS, Chan WN, Tan JR, Shamsuddin ZSB
    Polymers (Basel), 2021 Jul 13;13(14).
    PMID: 34301046 DOI: 10.3390/polym13142289
    As one of the fastest-growing additive manufacturing (AM) technologies, fused deposition modelling (FDM) shows great potential in printing natural fibre-reinforced composites (NFRC). However, several challenges, such as low mechanical properties and difficulty in printing, need to be overcome. Therefore, the effort to improve the NFRC for use in AM has been accelerating in recent years. This review attempts to summarise the current approaches of using NFRC as a feeder for AM. The effects of fibre treatments, composite preparation methods and addition of compatibilizer agents were analysed and discussed. Additionally, current methods of producing feeders from NFRCs were reviewed and discussed. Mechanical property of printed part was also dependent on the printing parameters, and thus the effects of printing temperature, layer height, infill and raster angle were discussed, and the best parameters reported by other researchers were identified. Following that, an overview of the mechanical properties of these composites as reported by various researchers was provided. Next, the use of optimisation techniques for NFRCs was discussed and analysed. Lastly, the review provided a critical discussion on the overall topic, identified all research gaps present in the use of NFRC for AM processes, and to overcome future challenges.
  2. Rajendran Royan NR, Sulong AB, Yuhana NY, Chen RS, Ab Ghani MH, Ahmad S
    PLoS One, 2018;13(5):e0197345.
    PMID: 29847568 DOI: 10.1371/journal.pone.0197345
    The use of rice husks (RH) to reinforce polymers in biocomposites are increasing tremendously. However, the incompatibility between the hydrophilic RH fibers and the hydrophobic thermoplastic matrices leads to unsatisfactory biocomposites. Surface modification of the fiber surface was carried out to improve the adhesion between fiber and matrix. In this study, the effect of surface modification of RH via alkali, acid and ultraviolet-ozonolysis (UV/O3) treatments on the properties of composites recycled high density polyethylene (rHDPE) composites was investigated. The untreated and treated RH were characterized by Fourier Transform Infrared (FTIR) and Scanning Electron Microscope (SEM). The composites containing 30 wt% of RH (treated and untreated) were then prepared via extrusion and followed by compression molding. As compared to untreated RH, all surface treated RH exhibited rougher surface and showed improved adhesion with rHDPE matrix. Tensile strength of UV/O3-treated RH composites showed an optimum result at 18.37 MPa which improved about 5% in comparison to the composites filled with untreated RH. UV/O3 treatment promotes shorter processing time and lesser raw material waste during treatment process where this is beneficial for commercialization in the future developments of wood plastic composites (WPCs). Therefore, UV/O3 treatment can be served as an alternative new method to modify RH surface in order to improve the adhesion between hydrophilic RH fibre and hydrophobic rHDPE polymer matrix.
  3. Mohd Radzuan NA, Khalid NN, Foudzi FM, Rajendran Royan NR, Sulong AB
    Polymers (Basel), 2023 Apr 11;15(8).
    PMID: 37111993 DOI: 10.3390/polym15081846
    The production of fabricated filaments for fused deposited modelling printing is critical, especially when higher loading filler (>20 wt.%) is involved. At higher loadings, printed samples tend to experience delamination, poor adhesion or even warping, causing their mechanical performance to deteriorate considerably. Hence, this study highlights the behaviour of the mechanical properties of printed polyamide-reinforced carbon fibre at a maximum of 40 wt.%, which can be improved via a post-drying process. The 20 wt.% samples also demonstrate improvements of 500% and 50% in impact strength and shear strength performance, respectively. These excellent performance levels are attributed to the maximum layup sequence during the printing process, which reduces the fibre breakage. Consequently, this enables better adhesion between layers and, ultimately, stronger samples.
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