Affiliations 

  • 1 Department of Chemistry, Faculty of Science, Universiti Malaya, 50603 Kuala Lumpur, Malaysia. Electronic address: ndiana13@um.edu.my
  • 2 Department of Chemistry, Faculty of Science, Universiti Malaya, 50603 Kuala Lumpur, Malaysia
  • 3 Department of Physics, Faculty of Science, Universiti Malaya, 50603 Kuala Lumpur, Malaysia
  • 4 Department of Engineering and Sciences, American Degree Program, School of Liberal Arts and Sciences, Taylor's University, Taylor's Lakeside Campus, No. 1 Jalan Taylor, 47500 Subang Jaya, Selangor, Malaysia. Electronic address: Nurfarhanim.AbuBakar@taylors.edu.my
Carbohydr Polym, 2025 Jan 15;348(Pt A):122830.
PMID: 39562104 DOI: 10.1016/j.carbpol.2024.122830

Abstract

This study investigates the preliminary efficacy of drug encapsulation in chitosan hydrogels by cathodic electrodeposition for the encapsulation of the aromatic dye methyl orange to enhance drug delivery in biological systems. Chitosan, a biocompatible and transparent polymer, is known for its ability to effectively encapsulate and transport therapeutic agents, which is critical for sustained and targeted drug release. Methyl orange was selected as a model drug to study the effects of deposition and immersion times on encapsulation efficiency. The effects of deposition and immersion times on encapsulation efficiency were analyzed by synthesizing multilayer hydrogels via electrochemical oxidation. Characterization techniques, including UV-visible spectroscopy, FTIR, and NMR, were employed; FTIR indicated an effective absorption of 4.34 % for Td50Ti60, while UV-Vis showed 46.41 % at Td60Ti50. NMR analysis revealed effective concentrations of 0.47 mM for Td70Ti60 and 0.38 mM for Td60Ti50, indicating that longer immersion times enhance absorption. These findings provide a foundation for further studies aimed at optimizing drug delivery strategies and improving the therapeutic efficacy of encapsulated agents in biological applications.

* Title and MeSH Headings from MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine.