Affiliations 

  • 1 Akdeniz University, Vocational School of Technical Sciences, Department of Electricity and Energy, Antalya, 07070, Turkey
  • 2 Akdeniz University, Vocational School of Health Services, Department of Medical Services and Techniques, Antalya, 07070, Turkey
  • 3 Department of Chemical and Environmental Engineering, Faculty of Science and Engineering, University of Nottingham Malaysia, Jalan Broga, Semenyih, 43500, Selangor Darul Ehsan, Malaysia
  • 4 School of Resources and Environment, University of Electronic Science and Technology of China, 611731, Xiyuan Ave, Chengdu, PR China; Department of Chemical Engineering, Quchan University of Technology, Quchan, 9477177870, Iran; Department of Chemical Sciences, University of Johannesburg, Doornfontein Campus, 2028 Johannesburg, 17011, South Africa. Electronic address: h.karimi.maleh@qiet.ac.ir
  • 5 Department of Chemical Engineering, Quchan University of Technology, Quchan, 9477177870, Iran
Chemosphere, 2022 Mar;290:133346.
PMID: 34929270 DOI: 10.1016/j.chemosphere.2021.133346

Abstract

Herein, it was aimed to optimize, model, and forecast the biosorption of Congo Red onto biomass-derived biosorbent. Therefore, the waste-orange-peels were processed to fabricate biomass-derived carbon, which was activated by ZnCl2 and modified with cetyltrimethylammonium bromide. The physicochemical properties of the biosorbents were explored by scanning electron microscopy and N2 adsorption/desorption isotherms. The effects of pH, initial dye concentration, temperature, and contact duration on the biosorption capacity were investigated and optimized by batch experimental process, followed by the kinetics, equilibrium, and thermodynamics of biosorption were modeled. Furthermore, various artificial neural network (ANN) architectures were applied to experimental data to optimize the ANN model. The kinetic modeling of the biosorption offered that biosorption was in accordance both with the pseudo-second-order and saturation-type kinetic model, and the monolayer biosorption capacity was calculated as 666.67 mg g-1 at 25 °C according to Langmuir isotherm model. According to equilibrium modeling, the Freundlich isotherm model was better fitted to the experimental data than the Langmuir isotherm model. Moreover, the thermodynamic modeling revealed biosorption took place spontaneously as an exothermic process. The findings revealed that the best ANN architecture trained with trainlm as the backpropagation algorithm, with tansig-purelin transfer functions, and 14 neurons in the single hidden layer with the highest coefficient of determination (R2 = 0.9996) and the lowest mean-squared-error (MSE = 0.0002). The well-agreement between the experimental and ANN-forecasted data demonstrated that the optimized ANN model can predict the behavior of the anionic dye biosorption onto biomass-derived modified carbon materials under various operation conditions.

* Title and MeSH Headings from MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine.