The mass attenuation coefficients of solid water phantoms, Perspex® phantoms and Rhizophora spp. particleboards were determined by using Compton scattering technique measured using Ludlum configuration. The gamma energy of 137Cs sealed source were measured at 30°, 45°, 60° and 75° angles providing scattered gamma energies between 337.72 and 564.09 keV. The mass attenuation coefficients of solid water and fabricated Rhizophora spp. particleboards were the nearest to XCOM values of water with average percentage of discrepancies of 6.8% and 5.9%, respectively. The results indicated similar attenuation properties of solid water and fabricated Rhizophora spp. particleboards and the suitability of the Ludlum configuration to determine the mass attenuation coefficient of materials using Compton scatter technique.