Affiliations 

  • 1 Department of Industrial and Production Engineering, Federal University of Technology, P.M.B.740 Akure, Nigeria. ngolaiya@futa.edu.ng
  • 2 Department of Chemical Engineering, Universitas Sumatera Utara, Medan 20155, Indonesia. indradanas@yahoo.com
  • 3 Department of Industrial and Production Engineering, Federal University of Technology, P.M.B.740 Akure, Nigeria. pkoke@futa.edu.ng
  • 4 Department of Mechanical Engineering, Universitas Syiah Kuala, Banda Aceh 23111, Indonesia. rizal@knt.mech.tut.ac.jp
  • 5 Department of Chemical, Metallurgical and Materials Engineering, Tshwane University of Technology, P.M.B. X680 Pretoria, South Africa. sadikur@tut.ac.za
  • 6 DST-/CSIR National Centre for Nanostructured Materials, Council for Scientific and Industrial Research, Pretoria 0001, South Africa. rsuprakas@csir.co.za
  • 7 Department of Industrial and Production Engineering, Federal University of Technology, P.M.B.740 Akure, Nigeria. pkfarayibi@futa.edu.ng
  • 8 School of Industrial Technology, Universiti Sains Malaysia,11800 Penang, Malaysia. sohrab@usm.my
  • 9 School of Industrial Technology, Universiti Sains Malaysia,11800 Penang, Malaysia. akhalilhps@gmail.com
Polymers (Basel), 2019 Oct 11;11(10).
PMID: 31614623 DOI: 10.3390/polym11101656

Abstract

This paper presents a comparison on the effects of blending chitin and/or starch with poly(lactic acid) (PLA). Three sets of composites (PLA-chitin, PLA-starch and PLA-chitin-starch) with 92%, 94%, 96% and 98% PLA by weight were prepared. The percentage weight (wt.%) amount of the chitin and starch incorporated ranges from 2% to 8%. The mechanical, dynamic mechanical, thermal and microstructural properties were analyzed. The results from the tensile strength, yield strength, Young's modulus, and impact showed that the PLA-chitin-starch blend has the best mechanical properties compared to PLA-chitin and PLA-starch blends. The dynamic mechanical analysis result shows a better damping property for PLA-chitin than PLA-chitin-starch and PLA-starch. On the other hand, the thermal property analysis from thermogravimetry analysis (TGA) shows no significant improvement in a specific order, but the glass transition temperature of the composite increased compared to that of neat PLA. However, the degradation process was found to start with PLA-chitin for all composites, which suggests an improvement in PLA degradation. Significantly, the morphological analysis revealed a uniform mix with an obvious blend network in the three composites. Interestingly, the network was more significant in the PLA-chitin-starch blend, which may be responsible for its significantly enhanced mechanical properties compared with PLA-chitin and PLA-starch samples.

* Title and MeSH Headings from MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine.