Browse publications by year: 2014

  1. Shaharudin S, Zanotto D, Agrawal S
    J Sports Sci Med, 2014 Dec;13(4):793-800.
    PMID: 25435771
    The slides ergometer (SE) was an improvisation from fixed ergometer (FE) to bridge the gap of mechanics between ergometer rowing and on-water rowing. The specific mechanical constraints of these two types of ergometers may affect the pattern of muscle recruitment, coordination and adaptation. The main purpose of this study was to evaluate the muscle synergy during 6 minutes maximal rowing on slides (SE) and fixed ergometers (FE). The laterality of muscle synergy was also examined. Surface electromyography activity, power output, heart rate, stroke length and stroke rate were analyzed from nine physically active subjects to assess the rowing performance. Physically active subjects, who were not specifically trained in rowing, were chosen to exclude the training effect on muscle synergy. Principal component analysis (PCA) with varimax rotation was applied to extract muscle synergy. Three muscle synergies were sufficient to explain the majority of variance in SE (94.4 ± 2.2 %) and FE (92.8 ± 1.7 %). Subjects covered more rowing distance, exerted greater power output and attained higher maximal heart rate during rowing on SE than on FE. The results proved the flexibility of muscle synergy to adapt to the mechanical constraints. Rowing on SE emphasized on bi-articular muscles contrary to rowing on FE which relied on cumulative effect of trunk and upper limb muscles during propulsive phase. Key pointsThree muscle synergies were extracted during maximal rowing on both fixed and slides ergometerUntrained subjects emphasized leg muscles while rowing on SEUntrained subjects focused on back muscles during FE rowing.
  2. Somchit MN, Sanat F, Hui GE, Wahab SI, Ahmad Z
    Adv Pharm Bull, 2014 Dec;4(4):401-4.
    PMID: 25436198 DOI: 10.5681/apb.2014.059
    PURPOSE: Nonsteroidal anti-inflammatory drugs (NSAIDs) are used for the treatment of many joint disorders, inflammation and to control pain. Numerous reports have indicated that NSAIDs are capable of producing nephrotoxicity in human. Therefore, the objective of this study was to evaluate mefenamic acid, a NSAID nephrotoxicity in an animal model.

    METHODS: Mice were dosed intraperitoneally with mefenamic acid either as a single dose (100 or 200 mg/kg in 10% Dimethyl sulfoxide/Palm oil) or as single daily doses for 14 days (50 or 100 mg/kg in 10% Dimethyl sulfoxide/Palm oil per day). Venous blood samples from mice during the dosing period were taken prior to and 14 days post-dosing from cardiac puncture into heparinized vials. Plasma blood urea nitrogen (BUN) and creatinine activities were measured.

    RESULTS: Single dose of mefenamic acid induced mild alteration of kidney histology mainly mild glomerular necrosis and tubular atrophy. Interestingly, chronic doses induced a dose dependent glomerular necrosis, massive degeneration, inflammation and tubular atrophy. Plasma blood urea nitrogen was statistically elevated in mice treated with mefenamic acid for 14 days similar to plasma creatinine.

    CONCLUSION: RESULTS from this study suggest that mefenamic acid as with other NSAIDs capable of producing nephrotoxicity. Therefore, the study of the exact mechanism of mefenamic acid induced severe nephrotoxicity can be done in this animal model.

    MeSH terms: Animals; Anti-Inflammatory Agents, Non-Steroidal; Atrophy; Blood Urea Nitrogen; Creatinine; Dimethyl Sulfoxide; Heparin; Humans; Inflammation; Kidney; Kidney Cortex Necrosis; Kidney Diseases; Kidney Glomerulus; Mefenamic Acid; Nitrogen; Pain; Punctures; Models, Animal; Mice
  3. Shani S, Ahmad RE, Naveen SV, Murali MR, Puvanan K, Abbas AA, et al.
    ScientificWorldJournal, 2014;2014:845293.
    PMID: 25436230 DOI: 10.1155/2014/845293
    Platelet rich concentrate (PRC) is a natural adjuvant that aids in human mesenchymal stromal cell (hMSC) proliferation in vitro; however, its role requires further exploration. This study was conducted to determine the optimal concentration of PRC required for achieving the maximal proliferation, and the need for activating the platelets to achieve this effect, and if PRC could independently induce early differentiation of hMSC. The gene expression of markers for osteocytes (ALP, RUNX2), chondrocytes (SOX9, COL2A1), and adipocytes (PPAR-γ) was determined at each time point in hMSC treated with 15% activated and nonactivated PRC since maximal proliferative effect was achieved at this concentration. The isolated PRC had approximately fourfold higher platelet count than whole blood. There was no significant difference in hMSC proliferation between the activated and nonactivated PRC. Only RUNX2 and SOX9 genes were upregulated throughout the 8 days. However, protein expression study showed formation of oil globules from day 4, significant increase in ALP at days 6 and 8 (P ≤ 0.05), and increased glycosaminoglycan levels at all time points (P < 0.05), suggesting the early differentiation of hMSC into osteogenic and adipogenic lineages. This study demonstrates that the use of PRC increased hMSC proliferation and induced early differentiation of hMSC into multiple mesenchymal lineages, without preactivation or addition of differentiation medium.
    MeSH terms: Blood Platelets/physiology*; Cell Differentiation/physiology*; Cells, Cultured; Humans; Cell Lineage/physiology*; Cell Proliferation/physiology*; Mesenchymal Stromal Cells/physiology*
  4. Chan XY, Chua KO, How KY, Yin WF, Chan KG
    ScientificWorldJournal, 2014;2014:930727.
    PMID: 25436236 DOI: 10.1155/2014/930727
    Most Pseudomonas putida strains are environmental microorganisms exhibiting a wide range of metabolic capability but certain strains have been reported as rare opportunistic pathogens and some emerged as multidrug resistant P. putida. This study aimed to assess the drug resistance profile of, via whole genome analysis, P. putida strain T2-2 isolated from oral cavity. At the same time, we also compared the nonenvironmental strain with environmentally isolated P. putida. In silico comparative genome analysis with available reference strains of P. putida shows that T2-2 has lesser gene counts on carbohydrate and aromatic compounds metabolisms, which suggested its little versatility. The detection of its edd gene also suggested T2-2's catabolism of glucose via ED pathway instead of EMP pathway. On the other hand, its drug resistance profile was observed via in silico gene prediction and most of the genes found were in agreement with drug-susceptibility testing in laboratory by automated VITEK 2. In addition, the finding of putative genes of multidrug resistance efflux pump and ATP-binding cassette transporters in this strain suggests a multidrug resistant phenotype. In summary, it is believed that multiple metabolic characteristics and drug resistance in P. putida strain T2-2 helped in its survival in human oral cavity.
    MeSH terms: Adaptation, Physiological/genetics*; Humans; Mouth/microbiology*; Genome, Bacterial/genetics*; Pseudomonas putida/genetics*; Drug Resistance, Multiple, Bacterial/genetics*; Comparative Genomic Hybridization/methods*
  5. Ullah S, Bustam MA, Nadeem M, Naz MY, Tan WL, Shariff AM
    ScientificWorldJournal, 2014;2014:940502.
    PMID: 25436237 DOI: 10.1155/2014/940502
    Melamine formaldehyde (MF) resins have been synthesized at different reaction temperature and pH values. Different molar ratios of melamine and formaldehyde were used to synthesize the corresponding resins. The prepared resin samples were characterized by using molecular weight determination viscometry and thermogravimetric analysis (TGA). The maximum percentage of solid content (69.7%) was obtained at pH 8.5 and 75°C temperature. The molecular weight of MF resin was increased with an increase of melamine monomer concentration. The highest residual weight 14.125 wt.% was obtained with sample 10.
    MeSH terms: Resins, Synthetic/chemical synthesis*; Resins, Synthetic/metabolism; Temperature*; Triazines/chemical synthesis*; Triazines/metabolism*
  6. Amiri M, Majid HA, Hairi F, Thangiah N, Bulgiba A, Su TT
    BMC Public Health, 2014;14 Suppl 3:S3.
    PMID: 25436515 DOI: 10.1186/1471-2458-14-S3-S3
    Objectives: The objectives are to assess the prevalence and determinants of cardiovascular disease (CVD) risk factors among the residents of Community Housing Projects in metropolitan Kuala Lumpur, Malaysia.
    Method: By using simple random sampling, we selected and surveyed 833 households which comprised of 3,722 individuals. Out of the 2,360 adults, 50.5% participated in blood sampling and anthropometric measurement sessions. Uni and bivariate data analysis and multivariate binary logistic regression were applied to identify demographic and socioeconomic determinants of the existence of having at least one CVD risk factor.
    Results: As a Result, while obesity (54.8%), hypercholesterolemia (51.5%), and hypertension (39.3%) were the most common CVD risk factors among the low-income respondents, smoking (16.3%), diabetes mellitus (7.8%) and alcohol consumption (1.4%) were the least prevalent. Finally, the results from the multivariate binary logistic model illustrated that compared to the Malays, the Indians were 41% less likely to have at least one of the CVD risk factors (OR = 0.59; 95% CI: 0.37 - 0.93).
    Conclusion: In Conclusion, the low-income individuals were at higher risk of developing CVDs. Prospective policies addressing preventive actions and increased awareness focusing on low-income communities are highly recommended and to consider age, gender, ethnic backgrounds, and occupation classes.
    MeSH terms: Adolescent; Adult; Alcohol Drinking/epidemiology; Cardiovascular Diseases/epidemiology*; Diabetes Mellitus/epidemiology; Female; Humans; Hypercholesterolemia/epidemiology; Hypertension/epidemiology; Malaysia/epidemiology; Male; Middle Aged; Obesity/epidemiology; Public Housing*; Risk Factors; Smoking/epidemiology; Socioeconomic Factors; Urban Health/statistics & numerical data*; Urban Population/statistics & numerical data*; Prevalence; Multivariate Analysis; Logistic Models; Young Adult
  7. Su TT, Majid HA, Nahar AM, Azizan NA, Hairi FM, Thangiah N, et al.
    BMC Public Health, 2014;14 Suppl 3:S4.
    PMID: 25436830 DOI: 10.1186/1471-2458-14-S3-S4
    Death rates due to hypertension in low and middle income countries are higher compared to high income countries. The present study is designed to combine life style modification and home blood pressure monitoring for control of hypertension in the context of low and middle income countries.
    MeSH terms: Adult; Behavior Therapy/methods*; Diet/psychology; Female; Follow-Up Studies; Humans; Hypertension/prevention & control*; Life Style*; Malaysia; Male; Motor Activity; Peer Group*; Social Support*; Health Behavior*; Cluster Analysis; Treatment Outcome; Blood Pressure Monitoring, Ambulatory/psychology*
  8. Hanifah RA, Majid HA, Jalaludin MY, Al-Sadat N, Murray LJ, Cantwell M, et al.
    BMC Public Health, 2014;14 Suppl 3:S5.
    PMID: 25436933 DOI: 10.1186/1471-2458-14-S3-S5
    The importance of fitness level on the well-being of children and adolescent has long been recognised. The aim of this study was to investigate the fitness level of school-going Malaysian adolescent, and its association with body composition indices.
    MeSH terms: Adolescent; Body Composition*; Cross-Sectional Studies; Female; Humans; Longitudinal Studies; Malaysia; Male; Physical Fitness/physiology*; Body Mass Index*; Waist Circumference*; Waist-Height Ratio*
  9. Hazreen MA, Su TT, Jalaludin MY, Dahlui M, Chinna K, Ismail M, et al.
    BMC Public Health, 2014;14 Suppl 3:S6.
    PMID: 25437068 DOI: 10.1186/1471-2458-14-S3-S6
    BACKGROUND: The National Health & Morbidity Survey (NHMS) IV (2011) observed that the prevalence of obese children aged less than 18 years in Malaysia is 6.1% compared to 5.4% overweight and obese in NHMS III (2006). As such, this observation is of public health importance as obesity is a forewarning risk factor for chronic diseases such as type-2 diabetes, cardiovascular diseases (CVD) and certain types of cancers. This MyHeART (Malaysian Health and Adolescents longitudinal Research Team) study aims to examine risk factors of non-communicable diseases (NCD) among adolescents.
    METHODS/DESIGN: The MyHeART study is longitudinal cohort study of 1361 schoolchildren (13-years old) attending 15 public secondary schools from the central (Kuala Lumpur and Selangor) and northern (Perak) regions of Peninsular Malaysia. The study used a stratified sampling design to select the study participants. Data collected at baseline included socio-economic, lifestyle (e.g. smoking, physical activity assessment, fitness assessment, seven-day diet history), and environmental information, anthropometric measurements, blood pressure, handgrip strength and bone mineral density. Blood samples for fasting blood glucose and lipid profiles, full blood count, renal profile, as well as bone profile and serum vitamin D were taken. This study cohort will be followed up again when participants turn 15, 17 and lastly, after a period of ten years (around the age of 27).
    RESULTS: Nine percent of the adolescents from this study were obese. More male participants smoked compared to female participants (15.4% vs. 4.7%). Adolescent males had higher fasting blood glucose but the female participants had lower high density lipoprotein (HDL-cholesterol) and higher low density lipoprotein (LDL-cholesterol). In addition, adolescents from the rural area had higher fasting blood glucose, diastolic blood pressure, total cholesterol and LDL-cholesterol.
    DISCUSSION: Our results demonstrated that adolescents from the rural area are at higher risk of NCDs compared to their urban counterpart. Tailor made public health interventions are highly recommended for adolescents as this may minimise the dreadful NCD burden in adulthood and health disparity between the rural and urban in the near future.
    Study name: Malaysian Health and Adolescents Longitudinal Research Team study (The MyHeART study)
    MeSH terms: Adolescent; Blood Glucose/analysis; Blood Pressure/physiology; Cardiovascular Diseases/epidemiology*; Diabetes Mellitus, Type 2/epidemiology*; Fasting/blood; Female; Health Surveys; Humans; Cholesterol, HDL/analysis; Cholesterol, LDL/analysis; Longitudinal Studies; Malaysia/epidemiology; Male; Neoplasms/epidemiology*; Risk Factors; Rural Population; Smoking/epidemiology; Prevalence; Sex Distribution; Pediatric Obesity/epidemiology*
  10. Fadzlina AA, Harun F, Nurul Haniza MY, Al Sadat N, Murray L, Cantwell MM, et al.
    BMC Public Health, 2014;14 Suppl 3:S7.
    PMID: 25437226 DOI: 10.1186/1471-2458-14-S3-S7
    BACKGROUND: Obesity and metabolic syndrome is prevalent among Malaysian adolescents and has been associated with certain behavioural factors such as duration of sleep, screen time and physical activity. The aim of the study is to report the prevalence of overweight/obesity, metabolic syndrome and its risk factors among adolescents.
    METHODS: A multi-staged cluster sampling method was used to select participants from urban and rural schools in Selangor, Perak and Wilayah Persekutuan Kuala Lumpur. Participants underwent anthropometric measurement and physical examination including blood pressure measurement. Blood samples were taken for fasting glucose and lipids and participants answered a self-administered questionnaire. Overweight and obesity was defined using the extrapolated adult body mass index (BMI) cut-offs of >25 kg/m2 and >30 kg/m2, according to the International Obesity Task Force (IOTF) criteria. Metabolic syndrome was defined based on International Diabetes Federation (IDF) 2007 criteria.
    RESULTS: Data were collected from 1361 participants. After excluding incomplete data and missing values for the variables, we analysed a sample of 1014 participants. Prevalence of overweight and obesity in this population was 25.4% (N = 258). The prevalence of metabolic syndrome was 2.6% in the population and 10% among the overweight and obese adolescents. Participants who slept between 7 and 9 hours a day has a lower risk of developing metabolic syndrome OR 0.38(0.15-0.94).
    CONCLUSION: Our results provide the prevalence of metabolic syndrome in Malaysian adolescents. Adequate sleep between 7 and 9 hours per day reduces the risk of developing metabolic syndrome.
    MESH: screen time
    MeSH terms: Adolescent; Female; Humans; Longitudinal Studies; Malaysia/epidemiology; Male; Risk Factors; Sleep; Time Factors; Prevalence; Risk Assessment; Metabolic Syndrome X/epidemiology*; Pediatric Obesity/epidemiology*
  11. Farid ND, Rus SC, Dahlui M, Al-Sadat N, Aziz NA
    BMC Public Health, 2014;14 Suppl 3(Suppl 3):S9.
    PMID: 25437631 DOI: 10.1186/1471-2458-14-S3-S9
    BACKGROUND: In welfare institutions, it is essential to address the health-related needs of adolescent populations who often engage in sexual activities. This study examines the association between individual and interpersonal factors concerning sexual risk behaviour (SRB) among adolescents in welfare institutions in Malaysia.

    METHODS: Data were derived from a cross-sectional study of 1082 adolescents in 22 welfare institutions located across Peninsular Malaysia in 2009. Using supervised self-administered questionnaires, adolescents were asked to assess their self-esteem and to complete questions on pubertal onset, substance use, family structure, family connectedness, parental monitoring, and peer pressure. SRB was measured through scoring of five items: sexual initiation, age of sexual debut, number of sexual partners, condom use, and sex with high-risk partners. Multivariate logistic regression analysis was used to examine the various predictors of sexual risk behaviour.

    RESULTS: The study showed that 55.1% (95%CI = 52.0-58.2) of the total sample was observed to practice sexual risk behaviours. Smoking was the strongest predictor of SRB among male adolescents (OR = 10.3, 95%CI = 1.25-83.9). Among females, high family connectedness (OR = 3.13, 95%CI = 1.64-5.95) seemed to predict the behaviour.

    CONCLUSION: There were clear gender differences in predicting SRB. Thus, a gender-specific sexual and reproductive health intervention for institutionalised adolescents is recommended.

    MeSH terms: Adolescent; Adolescent Behavior/psychology*; Child; Cross-Sectional Studies; Family Relations; Female; Humans; Malaysia/epidemiology; Male; Surveys and Questionnaires; Risk Factors; Risk-Taking*; Sexual Behavior/psychology*; Sexual Behavior/statistics & numerical data; Sex Factors; Smoking/epidemiology; Social Welfare*; Multivariate Analysis; Logistic Models; Young Adult
  12. Wong LP, Atefi N, Majid HA, Su TT
    BMC Public Health, 2014;14 Suppl 3(Suppl 3):S1.
    PMID: 25438066 DOI: 10.1186/1471-2458-14-S3-S1
    BACKGROUND: This study aimed to investigate the prevalence of pregnancy experience and its association with contraceptive knowledge among single adults in a low socio-economic suburban community in Kuala Lumpur, Malaysia.

    METHODS: A cross-sectional survey was conducted in 2012 among the Kerinchi suburban community. Of the total 3,716 individuals surveyed, young single adults between 18 and 35 years old were questioned with regard to their experience with unplanned pregnancy before marriage. Contraceptive knowledge was assessed by a series of questions on identification of method types and the affectivity of condoms for the prevention of sexually transmitted diseases.

    RESULTS: A total of 226 female and 257 male participants completed the survey. In total, eight female (3.5%) participants reported experience with an unplanned pregnancy before marriage, and five male (1.9 %) participants had the experience of impregnating their partners. The participants had a mean total score of 3.15 (SD = 1.55) for contraceptive knowledge out of a possible maximum score of five. Female participants who had experienced an unplanned pregnancy had a significantly lower contraceptive knowledge score (2.10 ± 1.48) than who had never experienced pregnancy (3.30 ± 1.35), p<0.05. Likewise, male participants who had experienced impregnating their partners had a significantly lower contraceptive knowledge score (1.60 ± 1.50) than those who did not have such experience (3.02 ± 1.59), p<0.05.

    CONCLUSION: The results showed evidence of premarital unplanned pregnancy among this suburban community. The low level of contraceptive knowledge found in this study indicates the need for educational strategies designed to improve contraceptive knowledge.

    MeSH terms: Adolescent; Adult; Cross-Sectional Studies; Female; Humans; Health Knowledge, Attitudes, Practice*; Malaysia/epidemiology; Male; Poverty Areas*; Pregnancy; Sexually Transmitted Diseases/prevention & control; Single Person/psychology*; Single Person/statistics & numerical data; Prevalence; Condoms/statistics & numerical data; Pregnancy, Unplanned*; Young Adult
  13. Jaafar N, Hakim H, Mohd Nor NA, Mohamed A, Saub R, Esa R, et al.
    BMC Public Health, 2014;14 Suppl 3:S2.
    PMID: 25438162 DOI: 10.1186/1471-2458-14-S3-S2
    The urban low income has often been assumed to have the greatest dental treatment needs compared to the general population. However, no studies have been carried out to verify these assumptions. This study was conducted to assess whether there was any difference between the treatment needs of an urban poor population as compared to the general population in order to design an intervention programme for this community.
    MeSH terms: Adult; Dental Care; Dental Caries/epidemiology*; Dental Health Surveys; Dentures/utilization*; Female; Humans; Malaysia/epidemiology; Male; Middle Aged; Periodontal Diseases/epidemiology*; Poverty Areas*; Temporomandibular Joint Disorders/epidemiology*; Urban Health/statistics & numerical data*; Prevalence; Cost of Illness*; Needs Assessment; Young Adult
  14. Azmi F, Ahmad Fuaad AA, Giddam AK, Batzloff MR, Good MF, Skwarczynski M, et al.
    Bioorg Med Chem, 2014 Nov 15;22(22):6401-8.
    PMID: 25438764 DOI: 10.1016/j.bmc.2014.09.042
    Peptides are of great interest to be used as vaccine antigens due to their safety, ease of manufacturing and specificity in generating immune response. There have been massive discoveries of peptide antigens over the past decade. However, peptides alone are poorly immunogenic, which demand co-administration with strong adjuvant to enhance their immunogenicity. Recently, fibril-forming peptides such as Q11 and lipoamino acid-based carrier have been identified to induce substantial immune responses when covalently linked to peptide epitope. In this study, we have incorporated either Q11 or lipoamino acids to a peptide epitope (J14) derived from M protein of group A streptococcus to develop self-adjuvanting vaccines. J14, Q11 and lipoamino acids were also conjugated together in a single vaccine construct in an attempt to evaluate the synergy effect of combining multiple adjuvants. Physicochemical characterization demonstrated that the vaccine constructs folded differently and self-assembled into nanoparticles. Significantly, only vaccine constructs containing double copies of lipoamino acids (regardless in conjugation with Q11 or not) were capable to induce significant dendritic cells uptake and subsequent J14-specific antibody responses in non-sizes dependent manners. Q11 had minimal impact in enhancing the immunogenicity of J14 even when it was used in combination with lipoamino acids. These findings highlight the impact of lipoamino acids moiety as a promising immunostimulant carrier and its number of attachment to peptide epitope was found to have a profound effect on the vaccine immunogenicity.
    MeSH terms: Adjuvants, Immunologic/chemistry*; Amino Acid Sequence; Animals; Epitopes/immunology; Epitopes/chemistry; Bacterial Proteins/chemistry; Circular Dichroism; Dendritic Cells/immunology; Dendritic Cells/metabolism; Enzyme-Linked Immunosorbent Assay; Female; Immunoglobulin G/analysis; Macrophages/immunology; Macrophages/metabolism; Molecular Sequence Data; Streptococcus pyogenes/metabolism*; Vaccines, Synthetic/immunology; Vaccines, Synthetic/chemistry*; Microscopy, Electron, Transmission; Mice; Lipopeptides/immunology; Lipopeptides/chemistry*
  15. Moniruzzaman M, Rodríguez I, Rodríguez-Cabo T, Cela R, Sulaiman SA, Gan SH
    J Chromatogr A, 2014 Nov 14;1368:26-36.
    PMID: 25441341 DOI: 10.1016/j.chroma.2014.09.057
    The suitability of the dispersive liquid-liquid microextraction (DLLME) technique for gas chromatography (GC) characterization of minor organic compounds in honey samples is evaluated. Under optimized conditions, samples were pre-treated by liquid-liquid extraction with acetonitrile followed by DLLME using carbon tetrachloride (CCl4, 0.075 mL) as extractant. The yielded settled phase was analyzed by GC using high resolution time-of-flight (TOF) mass spectrometry (MS). The whole sample preparation process is completed in approximately 10 min, with a total consumption of organic solvents below 4 mL, relative standard deviations lower than 12% and with more than 70 organic compounds, displaying linear retention index in the range from 990 to 2900, identified in the obtained extracts. In comparison with HS SPME extraction, higher peak intensities were attained for most volatile and semi-volatile compounds amenable to both extraction techniques. Furthermore, other species such as highly polar and water soluble benzene acids, long chain fatty acids, esters and flavonoids, which are difficult to concentrate by HS SPME, could be identified in DLLME extracts. Some of the compounds identified in DLLME extracts have been proposed as useful for samples classification and/or they are recognized as markers of honeys from certain geographic areas.
    MeSH terms: Honey/analysis*; Hydrogen-Ion Concentration; Gas Chromatography-Mass Spectrometry/methods*; Organic Chemicals/analysis*; Solvents/chemistry; Solid Phase Microextraction; Liquid Phase Microextraction/methods*
  16. Pan Y, Tiong KH, Abd-Rashid BA, Ismail Z, Ismail R, Mak JW, et al.
    Phytomedicine, 2014 Oct 15;21(12):1645-50.
    PMID: 25442272 DOI: 10.1016/j.phymed.2014.08.003
    This study was designed to investigate eight herbal active constituents (andrographolide, asiaticoside, asiatic acid, madecassic acid, eupatorin, sinensetin, caffeic acid, and rosmarinic acid) on their potential inhibitory effects on human cytochrome P450 1A2 (CYP1A2) activity. A fluorescence-based enzyme assay was performed by co-incubating human cDNA-expressed CYP1A2 with its selective probe substrate, 3-cyano-7-ethoxycoumarin (CEC), in the absence or presence of various concentrations of herbal active constituents. The metabolite (cyano-hydroxycoumarin) formed was subsequently measured in order to obtain IC50 values. The results indicated that only eupatorin and sinensetin moderately inhibited CYP1A2 with IC50 values of 50.8 and 40.2 μM, while the other active compounds did not significantly affect CYP1A2 activity with IC50 values more than 100 μM. Ki values further determined for eupatorin and sinensetin were 46.4 and 35.2 μM, respectively. Our data indicated that most of the investigated herbal constituents have negligible CYP1A2 inhibitory effect. In vivo studies however may be warranted to ascertain the inhibitory effect of eupatorin and sinensetin on CYP1A2 activity in clinical situations.
    MeSH terms: Flavonoids/pharmacology*; Humans; Plant Extracts/pharmacology*; Molecular Structure; Cytochrome P-450 CYP1A2/metabolism*; Inhibitory Concentration 50; Cytochrome P-450 CYP1A2 Inhibitors/pharmacology*
  17. Gan CY, Yoganathan K, Sim KS, Low YY, Lim SH, Kam TS
    Phytochemistry, 2014 Dec;108:234-42.
    PMID: 25442910 DOI: 10.1016/j.phytochem.2014.09.014
    Eleven indole alkaloids, comprising four corynanthean, two eburnane, one aspidofractinine, one secoleuconoxine, one andranginine, and two pauciflorine type alkaloids were isolated from the stem-bark and leaf extracts of Kopsia pauciflora. Their structures were determined using NMR and MS analyses. The catharinensine type alkaloid kopsirensine B and the secoleuconoxine alkaloid arboloscine A showed moderate to weak activity in reversing MDR in vincristine-resistant KB cells. The alkaloid content was markedly different compared to that of a sample from Malaysian Borneo.
    MeSH terms: Antineoplastic Agents, Phytogenic/isolation & purification*; Antineoplastic Agents, Phytogenic/pharmacology; Antineoplastic Agents, Phytogenic/chemistry; Drug Screening Assays, Antitumor; Humans; KB Cells; Lactams; Malaysia; Vincristine/pharmacology; Molecular Structure; Drug Resistance, Multiple/drug effects; Plant Leaves/chemistry; Drug Resistance, Neoplasm/drug effects; Nuclear Magnetic Resonance, Biomolecular; Plant Bark/chemistry; Indole Alkaloids/isolation & purification*; Indole Alkaloids/pharmacology; Indole Alkaloids/chemistry; Apocynaceae/chemistry*
  18. Chee Loong T, Idris A
    Bioresour Technol, 2014 Dec;174:311-5.
    PMID: 25443622 DOI: 10.1016/j.biortech.2014.10.015
    Biodiesel with improved yield was produced from microalgae biomass under simultaneous cooling and microwave heating (SCMH). Nannochloropsis sp. and Tetraselmis sp. which were known to contain higher lipid species were used. The yield obtained using this novel technique was compared with the conventional heating (CH) and microwave heating (MWH) as the control method. The results revealed that the yields obtained using the novel SCMH were higher; Nannochloropsis sp. (83.33%) and Tetraselmis sp. (77.14%) than the control methods. Maximum yields were obtained using SCMH when the microwave was set at 50°C, 800W, 16h of reaction with simultaneous cooling at 15°C; and water content and lipid to methanol ratio in reaction mixture was kept to 0 and 1:12 respectively. GC analysis depicted that the biodiesel produced from this technique has lower carbon components (<19 C) and has both reasonable CN and IV reflecting good ignition and lubricating properties.
    MeSH terms: Alkalies/pharmacology*; Biotechnology/methods*; Catalysis/drug effects; Esterification/drug effects; Esters/analysis; Fatty Acids/analysis; Heating*; Lipids/chemistry*; Microwaves*; Thermodynamics; Biofuels/microbiology*; Microalgae/metabolism*
  19. Subramanian P, Jayakumar M, Jayapalan JJ, Hashim OH
    Pharmacol Rep, 2014 Dec;66(6):1037-42.
    PMID: 25443732 DOI: 10.1016/j.pharep.2014.06.018
    BACKGROUND: Elevated blood ammonia leads to hyperammonaemia that affects vital central nervous system (CNS) functions. Fisetin, a naturally occurring flavonoid, exhibits therapeutic benefits, such as anti-cancer, anti-diabetic, anti-oxidant, anti-angiogenic, neuroprotective and neurotrophic effects.

    METHODS: In this study, the chronotherapeutic effect of fisetin on ammonium chloride (AC)-induced hyperammonaemic rats was investigated, to ascertain the time point at which the maximum drug effect is achieved. The anti-hyperammonaemic potential of fisetin (50mg/kg b.w. oral) was analysed when administered to AC treated (100mg/kg b.w. i.p.) rats at 06:00, 12:00, 18:00 and 00:00h. Amelioration of pathophysiological conditions by fisetin at different time points was measured by analysing the levels of expression of liver urea cycle enzymes (carbamoyl phosphate synthetase-I (CPS-I), ornithine transcarbamoylase (OTC) and argininosuccinate synthetase (ASS)), nuclear transcription factor kappaB (NF-κB p65), brain glutamine synthetase (GS) and inducible nitric oxide synthase (iNOS) by Western blot analysis.

    RESULTS: Fisetin increased the expression of CPS-I, OTC, ASS and GS and decreased iNOS and NF-κB p65 in hyperammonaemic rats. Fisetin administration at 00:00h showed more significant effects on the expression of liver and brain markers, compared with other time points.

    CONCLUSIONS: Fisetin could exhibit anti-hyperammonaemic effect owing to its anti-oxidant and cytoprotective influences. The temporal variation in the effect of fisetin could be due to the (i) chronopharmacological, chronopharmacokinetic properties of fisetin and (ii) modulations in the endogenous circadian rhythms of urea cycle enzymes, brain markers, redox enzymes and renal clearance during hyperammonaemia by fisetin. However, future studies in these lines are necessitated.

    MeSH terms: Ammonium Chloride/toxicity; Animals; Antioxidants/administration & dosage; Antioxidants/pharmacology; Brain/drug effects; Brain/metabolism; Flavonoids/administration & dosage; Flavonoids/pharmacology*; Inflammation/drug therapy; Inflammation/pathology; Liver/drug effects; Liver/metabolism; Time Factors; Urea/metabolism*; Blotting, Western; Biomarkers/metabolism; Hyperammonemia/drug therapy*; Rats; Drug Chronotherapy*
  20. Fornace KM, Drakeley CJ, William T, Espino F, Cox J
    Trends Parasitol, 2014 Nov;30(11):514-9.
    PMID: 25443854 DOI: 10.1016/j.pt.2014.09.001
    The potential applications of unmanned aerial vehicles (UAVs), or drones, have generated intense interest across many fields. UAVs offer the potential to collect detailed spatial information in real time at relatively low cost and are being used increasingly in conservation and ecological research. Within infectious disease epidemiology and public health research, UAVs can provide spatially and temporally accurate data critical to understanding the linkages between disease transmission and environmental factors. Using UAVs avoids many of the limitations associated with satellite data (e.g., long repeat times, cloud contamination, low spatial resolution). However, the practicalities of using UAVs for field research limit their use to specific applications and settings. UAVs fill a niche but do not replace existing remote-sensing methods.
    MeSH terms: Aircraft/standards*; Animals; Communicable Diseases/epidemiology*; Data Collection/instrumentation*; Humans; Malaria/epidemiology; Risk Factors; Spacecraft/standards; Remote Sensing Technology/standards
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