Displaying publications 1 - 20 of 47 in total

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  1. Fulltext Improved optimum condition for recovery and measurement of 210Po in environmental samples
    Zal U’yun Wan Mahmood, Norfaizal Mohamed @ Mohamad, Nik Azlin Nik Ariffin, Abdul Kadir Ishak
    Jurnal Sains Nuklear Malaysia, 2013;25(2):40-49.
    MyJurnal
    An improved laboratory technique for measurement of polonium-210(
    210Po) in environmental
    samples has been developed in Radiochemistry and Environmental Laboratory (RAS), Malaysian
    Nuclear Agency. To further improve this technique, a study with the objectives to determine the
    optimum conditions for
    210Po deposition and; evaluate the accuracy and precision results for
    the determination of 2 1 0 P o in environmental samples was carried-out. Polonium-210 which
    is an alpha emitter obtained in acidic solution through total digestion and dissolution of samples
    has been efficiently plated onto one side of the silver disc in the spontaneous plating process for
    measurement of its alpha activity. The optimum conditions for deposition of 210Po were achieved
    using hydrochloric acid (HCl) media at acidity of 0.5 M with the presence of 1.0 gram hydroxyl
    ammonium chloride and the plating temperature at 90
    oC. The plating was carried out in 80 mL
    HCl solution (0.5 M) for 4 hours. The recorded recoveries obtained using 2 0 9 P o tracers in
    the CRM IAEA-385 and environmental samples were 85% – 98% whereby the efficiency of the
    new technique is a distinct advantage over the existing techniques. Therefore, optimization of
    deposition parameters is a prime importance to achieve accuracy and precision results as well as
    economy and time saving
    Matched MeSH terms: Hydrochloric Acid
  2. Fulltext Evaluation of closed vessel microwave digestion of fish muscle with various solvent combinations using fractional factorial design
    Low, K.H., Zain, S.M., Abas, M.R., Ali Mohd, M.
    ASM Science Journal, 2009;3(1):71-76.
    MyJurnal
    Fractional factorial design was utilized to evaluate the effect of combinations of nitric acid, hydrogen peroxide, hydrochloric acid and water for microwave digestion of fish muscle. Upon digestion, copper, iron and zinc were determined by flame atomic absorption spectroscopy. H2O2 and HCl volumes were found to be the most significant parameters which resulted in good metal recoveries. This is especially so for the effect of HCl on Fe recovery. The results indicated that the combination of 4 mL 65% HNO3, 2 mL 30% H2O2 and 2 mL 30% HCl gave the most satisfactory percentage recovery. There was good agreement between measured and certified values for all metals with respect to the DORM-3 fish protein.
    Matched MeSH terms: Hydrochloric Acid
  3. Ultrasound mediated acid hydrolysis of konjac glucomannan
    Cheng, L.H., Nur Halawiah, H., Lai, B.N, Yong, H.M., Ang, S.L.
    International Food Research Journal, 2010;17(4):1043-1050.
    MyJurnal
    Konjac glucomannan (KGM) was treated with or without sonication and/or hydrochloric acid (HCl).
    Hydrolysis effects on KGM were studied for properties such as degree of hydrolysis, fluidity, molecular mass, and creep properties. The degree of hydrolysis for sonicated KGM and acid treated KGM were not significantly different. However, the combination treatment of acid hydrolysis and sonication was found effective in yielding a smaller molecular weight fraction of KGM and solution with higher fluidity. From the creep analysis, KGM treated with combination treatment exhibited the highest compliance among samples tested. In general, ultrasound mediated acid hydrolysis was found to be a promising technique in degrading high molecular weight biopolymer. This could be attributed to a localized high temperature and high shear forces generated during cavitation that facilitated the endothermic acid hydrolysis.
    Matched MeSH terms: Hydrochloric Acid
  4. Fulltext Ime course detachment of biofilms in pipes by hydrochlorination
    Shanzay, A., Siddra, T. A., Warda, F., Sheeza, A., Maryam, A., Aina, S. Z., et al.
    Asian Journal of Medicine and Biomedicine, 2018;1(1):28-31.
    MyJurnal
    Bacterial biofilms are a complex community of microbes in which the cells are embedded in a polysaccharide matrix.
    This slime is a mean of protection in hostile environments. Biofilms in hospital settings are perilous as they not only
    make treatment difficult, cause blockage of pipes but are also cause of serious nosocomial infections thus making their
    dispersal an even more important phenomenon. Any foaming method is not applicable at all places for the cleaning of
    biofilms hence biofilm dispersal by household sweep containing hydrochloric acid was checked using the microliter
    plate assay as dispersal strategy. Bacteria from hospital waste disposal pipes were isolated, its ability to form biofilm
    was noted under different time intervals and then finally biofilm degradation was done using different concentrations
    of household sweep. It was noted that household sweep can be successfully employed at many places especially waste
    disposal pipes and acid resistant tubes. Our results indicated that 20% sweep (HCl conc. 1%) if used for only one
    minute can reduce the biofilms to 50%. Similarly increasing contact time can reduce the biofilms further.
    Matched MeSH terms: Hydrochloric Acid
  5. Fulltext Comparative chemical characteristics of hydrochloric acid- and ammonium oxalate-extracted pectin from roselle (Hibiscus sabdariffa L.) calyces
    Nazaruddin, R., Noor Baiti, A.A., Foo, S.C., Tan, Y.N., Ayob, M.K.
    International Food Research Journal, 2013;20(1):281-284.
    MyJurnal
    Recent research suggesting the existence of potential source of pectin from roselle calyces. Pectin was successfully extracted from seven different varieties of roselle calyces. Pectin extraction was conducted using hydrochloric acid (HCl, 0.03 N, pH 1.5) or ammonium oxalate (0.25% w/v, pH 4.6) at 85⁰C for 1 h. Chemical characteristics of the HCl- and ammonium oxalate extracted pectin were compared. Results indicated that ammonium oxalate exhibited greater efficiency in pectin extraction than HCl. Highest pectin yield at 18.7% was obtained by ammonium oxalate extraction of roselle calyx variety Acc.6 compared to only 9.77% by HCl extraction. The lowest pectin yield at 11.3% and 5.78% were observed respectively in ammonium oxalate and HCl extractions of roselle calyx variety UKMR-3. Some important characteristics of ammonium oxalate extracted pectin of roselle Acc.6 were 5.98% moisture, 3.81% ash, 4.64% methoxyl content, 42.24% anhydrouronic acid (AUA) and degree of esterification (DE) 60%. This study suggested that the high DE% roselle pectin is an alternative source of pectin for food industry.
    Matched MeSH terms: Hydrochloric Acid
  6. Enhanced fermentable sugar production from kitchen waste using various pretreatments
    Hafid HS, Rahman NA, Md Shah UK, Baharudin AS
    J Environ Manage, 2015 Jun 1;156:290-8.
    PMID: 25900092 DOI: 10.1016/j.jenvman.2015.03.045
    The kitchen waste fraction in municipal solid waste contains high organic matter particularly carbohydrate that can contribute to fermentable sugar production for subsequent conversion to bioethanol. This study was carried out to evaluate the influence of single and combination pretreatments of kitchen waste by liquid hot water, mild acid pretreatment of hydrochloric acid (HCl) and sulphuric acid (H2SO4) and enzymatic hydrolysis (glucoamylase). The maximum total fermentable sugar produced after combination pretreatment by 1.5% HCl and glucoamylase consisted of 93.25 g/L glucose, 0.542 g/L sucrose, 0.348 g/L maltose, and 0.321 g/L fructose. The glucose released by the combination pretreatment method was 0.79 g glucose/g KW equivalent to 79% of glucose conversion. The effects of the pre-treatment on kitchen waste indicated that the highest solubilization was 40% by the combination method of 1.5% HCl and glucoamylase. The best combination pre-treatment gave concentrations of lactic acid, acetic acid, and propionic acid of 11.74 g/L, 6.77 g/L, and 1.02 g/L, respectively. The decrease of aliphatic absorbance bands of polysaccharides at 2851 and 2923 cm(-1) and the increase on structures of carbonyl absorbance bands at 1600 cm(-1) reflects the progress of the kitchen waste hydrolysis to fermentable sugars. Overall, 1.5% HCl and glucoamylase treatment was the most profitable process as the minimum selling price of glucose was USD 0.101/g kitchen waste. Therefore, the combination pretreatment method was proposed to enhance the production of fermentable sugar, particularly glucose from kitchen waste as the feedstock for bioethanol production.
    Matched MeSH terms: Hydrochloric Acid/chemistry
  7. Fulltext A visual tutorial on the synthesis of gold nanoparticles
    Low A, Bansal V
    Biomed Imaging Interv J, 2010 01 01;6(1):e9.
    PMID: 21611068 DOI: 10.2349/biij.6.1.e9
    Many papers have been written on the synthesis of gold nanoparticles but very few included pictures of the process, and none of them used video to show the whole process of synthesis. This paper records the process of synthesis of gold nanoparticles using video clips. Every process from cleaning of glassware, an important step in the synthesis of metallic nanoparticles, to the dialysis process is shown. It also includes the preparation of aqua regia and the actual synthesis of gold nanoparticles. In some papers, the dialysis process was omitted, but in this paper, it is included to complete the whole process as it is being used for purification.
    Matched MeSH terms: Hydrochloric Acid
  8. Optimization of cell disruption methods for efficient recovery of bioactive metabolites via NMR of three freshwater microalgae (chlorophyta)
    Ma NL, Teh KY, Lam SS, Kaben AM, Cha TS
    Bioresour Technol, 2015 Aug;190:536-42.
    PMID: 25812996 DOI: 10.1016/j.biortech.2015.03.036
    This study demonstrates the use of NMR techniques coupled with chemometric analysis as a high throughput data mining method to identify and examine the efficiency of different disruption techniques tested on microalgae (Chlorella variabilis, Scenedesmus regularis and Ankistrodesmus gracilis). The yield and chemical diversity from the disruptions together with the effects of pre-oven and pre-freeze drying prior to disruption techniques were discussed. HCl extraction showed the highest recovery of oil compounds from the disrupted microalgae (up to 90%). In contrast, NMR analysis showed the highest intensity of bioactive metabolites obtained for homogenized extracts pre-treated with freeze-drying, indicating that homogenizing is a more favorable approach to recover bioactive substances from the disrupted microalgae. The results show the potential of NMR as a useful metabolic fingerprinting tool for assessing compound diversity in complex microalgae extracts.
    Matched MeSH terms: Hydrochloric Acid/chemistry*
  9. Syk/NF-κB-targeted anti-inflammatory activity of Melicope accedens (Blume) T.G. Hartley methanol extract
    Kim JK, Choi E, Hong YH, Kim H, Jang YJ, Lee JS, et al.
    J Ethnopharmacol, 2021 May 10;271:113887.
    PMID: 33539951 DOI: 10.1016/j.jep.2021.113887
    ETHNOPHARMACOLOGICAL RELEVANCE: Melicope accedens (Blume) Thomas G. Hartley is a plant included in the family Rutaceae and genus Melicope. It is a native plant from Vietnam that has been used for ethnopharmacology. In Indonesia and Malaysia, the leaves of M. accedens are applied externally to decrease fever.

    AIM OF THE STUDY: The molecular mechanisms of the anti-inflammatory properties of M. accedens are not yet understood. Therefore, we examined those mechanisms using a methanol extract of M. accedens (Ma-ME) and determined the target molecule in macrophages.

    MATERIALS AND METHODS: We evaluated the anti-inflammatory effects of Ma-ME in lipopolysaccharide (LPS)-stimulated RAW264.7 cells and in an HCl/EtOH-triggered gastritis model in mice. To investigate the anti-inflammatory activity, we performed a nitric oxide (NO) production assay and ELISA assay for prostaglandin E2 (PGE2). RT-PCR, luciferase gene reporter assays, western blotting analyses, and a cellular thermal shift assay (CETSA) were conducted to identify the mechanism and target molecule of Ma-ME. The phytochemical composition of Ma-ME was analyzed by HPLC and LC-MS/MS.

    RESULTS: Ma-ME suppressed the production of NO and PGE2 and the mRNA expression of proinflammatory genes (iNOS, IL-1β, and COX-2) in LPS-stimulated RAW264.7 cells without cytotoxicity. Ma-ME inhibited NF-κB activation by suppressing signaling molecules such as IκBα, Akt, Src, and Syk. Moreover, the CETSA assay revealed that Ma-ME binds to Syk, the most upstream molecule in the NF-κB signal pathway. Oral administration of Ma-ME not only alleviated inflammatory lesions, but also reduced the gene expression of IL-1β and p-Syk in mice with HCl/EtOH-induced gastritis. HPLC and LC-MS/MS analyses confirmed that Ma-ME contains various anti-inflammatory flavonoids, including quercetin, daidzein, and nevadensin.

    CONCLUSIONS: Ma-ME exhibited anti-inflammatory activities in vitro and in vivo by targeting Syk in the NF-κB signaling pathway. Therefore, we propose that Ma-ME could be used to treat inflammatory diseases such as gastritis.

    Matched MeSH terms: Hydrochloric Acid/toxicity
  10. Determination of silver, bismuth, cadmium, copper, iron, nickel and zinc in lead- and tin-base solders and white-metal bearing alloys by atomic-absorption spectrophotometry
    Chong C
    Talanta, 1986 Jan;33(1):91-4.
    PMID: 18964038
    A simple atomic-absorption spectrophotometry method is described for the determination of silver, bismuth, cadmium, copper, iron, nickel and zinc in lead- and tin-base solders and white-metal bearing alloys, with use of a single sample solution. The sample is dissolved in a mixture of hydrobromic acid and bromine, then fumed with sulphuric acid. The lead sulphate is dissolved in concentrated hydrochloric acid. The method is particularly suitable for the determination of silver and bismuth, which are co-precipitated with lead sulphate. The other elements can also be determined after removal of the lead sulphate by filtration.
    Matched MeSH terms: Hydrochloric Acid
  11. New One-Pot Synthesis of 1,3,5-Triazines: Three-Component Condensation, Dimroth Rearrangement, and Dehydrogenative Aromatization
    Junaid A, Lim FPL, Tiekink ERT, Dolzhenko AV
    ACS Comb Sci, 2019 07 08;21(7):548-555.
    PMID: 31180634 DOI: 10.1021/acscombsci.9b00079
    A new, effective one-pot synthesis of the 6, N2-diaryl-1,3,5-triazine-2,4-diamines under microwave irradiation was developed. The method involved an initial three-component condensation of cyanoguanidine, aromatic aldehydes, and arylamines in the presence of hydrochloric acid. Without isolation, the resulting 1,6-diaryl-1,6-dihydro-1,3,5-triazine-2,4-diamines were treated with a base to initiate Dimroth rearrangement and spontaneous dehydrogenative aromatization, affording the desired compounds. The developed method was found to be sufficiently general in scope, tolerating various aromatic aldehydes and amines; by using their combinations in the first step, a representative library of 110 compounds was successfully prepared and screened for anticancer properties.
    Matched MeSH terms: Hydrochloric Acid/pharmacology*; Hydrochloric Acid/chemistry
  12. Fulltext A Zinc Morpholine Complex Prevents HCl/Ethanol-Induced Gastric Ulcers in a Rat Model
    Salama SM, Gwaram NS, AlRashdi AS, Khalifa SA, Abdulla MA, Ali HM, et al.
    Sci Rep, 2016 07 27;6:29646.
    PMID: 27460157 DOI: 10.1038/srep29646
    Zinc is a naturally occurring element with roles in wound healing and rescuing tissue integrity, particularly in the gastrointestinal system, where it can be detected in the mucosal and submucosal layers. Zinc chelates are known to have beneficial effects on the gastrointestinal mucosa and in cases of gastric ulcer. We synthesized complexes of zinc featuring a heterocyclic amine binding amino acids then investigated their ability to enhance the gastric self-repair. Zinc-morpholine complex, Zn(L)SCN, namely showed strong free-radical scavenging, promotion of the DNA and RNA polymerases reconstruction and suppression of cell damage. The complex's mode of action is proposed to involve hydrogen bond formation via its bis(thiocyanato-k)zinc moiety. Zn(L)SCN complex had potent effects on gastric enzymatic activity both in vitro and in vivo. The complex disrupted the ulcerative process as demonstrated by changes in the intermediate metabolites of the oxidative pathway - specifically, reduction in the MDA levels and elevation of reduced glutathione together with an attenuation of oxidative DNA damage. Additionally, Zn(L)SCN restored the gastric mucosa, inhibited the production of pro-inflammatory cytokines (IL-6, TNF and the caspases), and preserved the gastric mucous balance. Zn(L)SCN thus exhibited anti-oxidative, anti-inflammatory and anti-apoptotic activities, all of which have cytoprotective effects on the gastric lining.
    Matched MeSH terms: Hydrochloric Acid/adverse effects*
  13. Influence of alkaline hydrogen peroxide pre-hydrolysis on the isolation of microcrystalline cellulose from oil palm fronds
    Owolabi AF, Haafiz MK, Hossain MS, Hussin MH, Fazita MR
    Int J Biol Macromol, 2017 Feb;95:1228-1234.
    PMID: 27836655 DOI: 10.1016/j.ijbiomac.2016.11.016
    In the present study, microcrystalline cellulose (MCC) was isolated from oil palm fronds (OPF) using chemo-mechanical process. Wherein, alkaline hydrogen peroxide (AHP) was utilized to extract OPF fibre at different AHP concentrations. The OPF pulp fibre was then bleached with acidified sodium chlorite solution followed by the acid hydrolysis using hydrochloric acid. Several analytical methods were conducted to determine the influence of AHP concentration on thermal properties, morphological properties, microscopic and crystalline behaviour of isolated MCC. Results showed that the MCC extracted from OPF fibres had fibre diameters of 7.55-9.11nm. X-ray diffraction (XRD) analyses revealed that the obtained microcrystalline fibre had both celluloses I and cellulose II polymorphs structure, depending on the AHP concentrations. The Fourier transmission infrared (FTIR) analyses showed that the AHP pre-hydrolysis was successfully removed hemicelluloses and lignin from the OPF fibre. The crystallinity of the MCC was increased with the AHP concentrations. The degradation temperature of MCC was about 300°C. The finding of the present study showed that pre-treatment process potentially influenced the quality of the isolation of MCC from oil palm fronds.
    Matched MeSH terms: Hydrochloric Acid/chemistry
  14. Insights into the equilibrium, kinetic and thermodynamics of nickel removal by environmental friendly Lansium domesticum peel biosorbent
    Lam YF, Lee LY, Chua SJ, Lim SS, Gan S
    Ecotoxicol Environ Saf, 2016 May;127:61-70.
    PMID: 26802563 DOI: 10.1016/j.ecoenv.2016.01.003
    Lansium domesticum peel (LDP), a waste material generated from the fruit consumption, was evaluated as a biosorbent for nickel removal from aqueous media. The effects of dosage, contact time, initial pH, initial concentration and temperature on the biosorption process were investigated in batch experiments. Equilibrium data were fitted by the Langmuir, Freundlich, Temkin and Dubinin-Radushkevich models using nonlinear regression method with the best-fit model evaluated based on coefficient of determination (R(2)) and Chi-square (χ(2)). The best-fit isotherm was found to be the Langmuir model exhibiting R(2) very close to unity (0.997-0.999), smallest χ(2) (0.0138-0.0562) and largest biosorption capacity (10.1mg/g) at 30°C. Kinetic studies showed that the initial nickel removal was rapid with the equilibrium state established within 30min. Pseudo-second-order model was the best-fit kinetic model indicating the chemisorption nature of the biosorption process. Further data analysis by the intraparticle diffusion model revealed the involvement of several rate-controlling steps such as boundary layer and intraparticle diffusion. Thermodynamically, the process was exothermic, spontaneous and feasible. Regeneration studies indicated that LDP biosorbent could be regenerated using hydrochloric acid solution with up to 85% efficiency. The present investigation proved that LDP having no economic value can be used as an alternative eco-friendly biosorbent for remediation of nickel contaminated water.
    Matched MeSH terms: Hydrochloric Acid
  15. Non-erosive reflux disease (NERD), symptomatic and asymptomatic erosive reflux disease (ERD): from hypersensitive to hyposensitive esophagus
    Hartono JL, Qua CS, Goh KL
    Dig Dis Sci, 2011 Jan;56(1):90-6.
    PMID: 20467897 DOI: 10.1007/s10620-010-1275-5
    AIMS: To compare the esophageal sensitivity to acid and saline in patients with symptomatic and asymptomatic erosive reflux disease (ERD), non-erosive reflux disease (NERD) and controls, and to assess the response to proton-pump inhibitors in patients with symptomatic ERD and NERD.

    METHODOLOGY: Patients with GERD and a control group of healthy asymptomatic volunteers were recruited. All subjects underwent esophagogastroduodenoscopy and the acid-saline perfusion test. Symptomatic ERD and NERD patients were given rabeprazole 20 mg twice daily for 2 weeks and their response to treatment assessed.

    RESULTS: A total of 105 subjects were recruited: ERD=37 (symptomatic=24, asymptomatic=13), NERD=34 and controls=34. During saline perfusion, only the NERD group recorded a significantly higher sensitivity score compared to controls (2.74±7.28 vs. 0) (p=0.035). During acid perfusion, symptomatic ERD (15.42±13.42) and NERD (16.71±15.04) had significantly higher scores versus controls and asymptomatic ERD patients (both p<0.001). The mean %∆ reflux symptom score following treatment was significantly higher in symptomatic ERD patients compared to NERD patients (89.08±21.67 vs. 58.53±32.54; p<0.001).

    CONCLUSIONS: Patients with NERD were a generally hypersensitive group while asymptomatic ERD patients represent a hyposensitive group of patients which merits further study.

    Matched MeSH terms: Hydrochloric Acid/adverse effects
  16. Biosorption of copper ions from dilute aqueous solutions on base treated rubber (Hevea brasiliensis) leaves powder: kinetics, isotherm, and biosorption mechanisms
    Wan Ngah WS, Hanafiah MA
    J Environ Sci (China), 2008;20(10):1168-76.
    PMID: 19143339
    The efficiency of sodium hydroxide treated rubber (Hevea brasiliensis) leaves powder (NHBL) for removing copper ions from aqueous solutions has been investigated. The effects of physicochemical parameters on biosorption capacities such as stirring speed, pH, biosorbent dose, initial concentrations of copper, and ionic strength were studied. The biosorption capacities of NHBL increased with increase in pH, stirring speed and copper concentration but decreased with increase in biosorbent dose and ionic strength. The isotherm study indicated that NHBL fitted well with Langmuir model compared to Freundlich and Dubinin-Radushkevich models. The maximum biosorption capacity determined from Langmuir isotherm was 14.97 mg/g at 27 degrees C. The kinetic study revealed that pseudosecond order model fitted well the kinetic data, while Boyd kinetic model indicated that film diffusion was the main rate determining step in biosorption process. Based on surface area analysis, NHBL has low surface area and categorized as macroporous. Fourier transform infrared (FT-IR) analyses revealed that hydroxyl, carboxyl, and amino are the main functional groups involved in the binding of copper ions. Complexation was one of the main mechanisms for the removal of copper ions as indicated by FT-IR spectra. Ion exchange was another possible mechanism since the ratio of adsorbed cations (Cu2+ and H+) to the released cations (Na+, Ca2+, and Mg2+) from NHBL was almost unity. Copper ions bound on NHBL were able to be desorbed at > 99% using 0.05 mol/L HCl, 0.01 mol/L HNO3, and 0.01 mol/L EDTA solutions.
    Matched MeSH terms: Hydrochloric Acid/chemistry
  17. Restoration of engraved marks on steel surfaces by etching technique
    Zaili MA, Kuppuswamy R, Harun H
    Forensic Sci Int, 2007 Aug 24;171(1):27-32.
    PMID: 17088038
    It is known that restoration of erased engraved identification marks on the engine and the chassis of a car or on a firearm has low success rate. Unlike stamping, engraving on a metal surface leaves no pronounced, permanent subsurface deformation in the crystalline structure, also called dislocation that can be revealed by suitable methods. Hence, the current research work investigated whether metallographic reagents used in the restoration of stamp (compression) marks could be applied to recover engraved marks on steel surfaces and also to establish the sensitivity and effectiveness of some of these reagents for the restoration of the marks. Experiments were conducted by mechanically engraving alphanumeric characters on several steel plates using a computer controlled engraving machine called Gravograph. The markings were later erased from the above steel plates by removing the metal in stages of 0.01 mm through 0.04 mm below the bottom of the engraving. Several plates were thus prepared wherein each one had been abraded to a specific depth. Then eight metallographic reagents were tested on each one of the above erased plates using a swabbing technique. The results had shown that while most of the reagents were able to restore marks up to certain levels of erasure, the reagent 5 g copper sulphate, 60 ml water, 30 ml concentrated ammonium hydroxide and 60 ml concentrated hydrochloric acid restored marks erased to a depth of 0.04 mm below the engraving depth, thus presenting itself the most sensitive reagent. Quite significantly, the above reagent was also able to decipher successfully the original engraved marks that had been erased and engraved with a new number, or obliterated by centre punching. The results of this research work should benefit the forensic practitioners engaged in the serial number recovery on vehicles, firearms and other objects.
    Matched MeSH terms: Hydrochloric Acid
  18. Dynamic supported liquid membrane tip extraction of glyphosate and aminomethylphosphonic acid followed by capillary electrophoresis with contactless conductivity detection
    See HH, Hauser PC, Sanagi MM, Ibrahim WA
    J Chromatogr A, 2010 Sep 10;1217(37):5832-8.
    PMID: 20696433 DOI: 10.1016/j.chroma.2010.07.054
    A dynamic supported liquid membrane tip extraction (SLMTE) procedure for the effective extraction and preconcentration of glyphosate (GLYP) and its metabolite aminomethylphosphonic acid (AMPA) in water has been investigated. The SLMTE procedure was performed in a semi-automated dynamic mode and demonstrated a greater performance against a static extraction. Several important extraction parameters such as donor phase pH, cationic carrier concentration, type of membrane solvent, type of acceptor stripping phase, agitation and extraction time were comprehensively optimized. A solution of Aliquat-336, a cationic carrier, in dihexyl ether was selected as the supported liquid incorporated into the membrane phase. Quantification of GLYP and AMPA was carried out using capillary electrophoresis with contactless conductivity detection. An electrolyte solution consisting of 12 mM histidine (His), 8 mM 2-(N-morpholino)ethanesulfonic acid (MES), 75 microM cetyltrimethylammonium bromide (CTAB), 3% methanol, pH 6.3, was used as running buffer. Under the optimum extraction conditions, the method showed good linearity in the range of 0.01-200 microg/L (GLYP) and 0.1-400 microg/L (AMPA), acceptable reproducibility (RSD 5-7%, n=5), low limits of detection of 0.005 microg/L for GLYP and 0.06 microg/L for AMPA, and satisfactory relative recoveries (90-94%). Due to the low cost, the SLMTE device was disposed after each run which additionally eliminated the possibility of carry-over between runs. The validated method was tested for the analysis of both analytes in spiked tap water and river water with good success.
    Matched MeSH terms: Hydrochloric Acid/chemistry
  19. Fulltext Characterization and functional properties of gelatin extracted from goatskin
    Zilhadia, Yahdiana,H., Effionora, A., Irwandi, J.
    International Food Research Journal, 2018;25(1):275-281.
    MyJurnal
    Gelatin from goatskin pretreated with hydrochloric acid and extracted with distilled water at 60oC for 9 hours was characterized and compared to that of bovine skin gelatin (BSG). A yield of 10.26% (wet weight basis) was obtained. Goatskin gelatin (GSG) had high protein (86.58%), suitable moisture (9.58%), low fat (1.46%) and low ash (0.11%) content. The functional properties of GSG including gel strength (301 g bloom) and emulsion activity index (94.27%) were higher than the functional properties of BSG including gel strength (192 g bloom) and emulsion activity index (49.74%). The foaming property of GSG (102%) was lower than that of BSG (164.67%). This study shows that GSG has a high potential for application as a source of commercial gelatin.
    Matched MeSH terms: Hydrochloric Acid
  20. Fulltext Corrosion behaviour of Al-Si cast alloy reinforced with titanium diboride (TiB2) and scandium (Sc)
    Ibrahim, R.E., Talari, M.K., Sabrina, M. Yahaya, Rosmamuhamadani, R., Sulaiman, S., Ismail, M.I.S.
    Journal of Engineering and Science Research, 2018;2(2):1-8.
    MyJurnal
    The aluminium-silicon (Al-Si) based on Metal Matrix Composites (MMCs) is widely used in lightweight
    constructions and transport applications requiring a combination of high strength and ductility. A grain
    refinement plays a crucial role in improving characteristics and properties of Al alloys. In this investigation,
    titanium diboride (TiB2) and scandium (Sc) inoculants were added to the Al-Si alloys for grain refinement of
    an alloy. In this investigation, the corrosion resistance rate of Al-Si cast alloy reinforced by TiB2 and Sc were
    measured by potentiostat (AUTOLAB) instrument. The aim of this research is to investigate the corrosion
    rate for Al-Si-TiB2-Sc composites that immersed in different concentration of acidic solutions. Besides, the
    immersion time of acidic solutions also was investigated. All the samples were prepared accordingly for
    ASTM standard by the composition of 6.0 wt% TiB2 and 0.6wt% Sc. All the samples undergo cold mounting
    technique for easy handling on corrosion tests. Then the samples were immersed in two different
    concentrations acidic medium solutions, which were 0.1.and 1.0 M hydrochloric acids (HCl). The corrosion
    rate also was investigated for immersion samples of 1.0 M HCl for 21 days. From the results obtained, added
    TiB2 and Sc onto Al-Si alloy gave the better properties in corrosion resistance. Corrosion rates to reduce when
    the samples were immersed in a lower concentration of acidic medium, 0.1 HCl. However, there are some
    significant on the result but it still following the corrosion rates trend. Thus, improvements to reinforcement
    content need to be done in further research to cover the lack of this corrosion rates trend.
    Matched MeSH terms: Hydrochloric Acid
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